Synthesis and Characterization of Nanostructure BPO4 |
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| Authors: | Shuang Chen Ming Ye Hao-Hong Chen Xin-Xin Yang Jing-Tai Zhao |
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| Affiliation: | (1) State Key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai, 200050, People’s Republic of China;(2) Graduate School of Chinese Academy of Sciences, Beijing, People’s Republic of China;(3) Single Molecule Detecting and Manipulating Lab, Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai, People’s Republic of China |
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| Abstract: | Boron phosphate (BPO4) is a well known catalyst for a range of organic chemical reactions. In this paper, we report the preparations and characterizations
of nano-sized BPO4 and nano-BPO4-based core-shell spheres. The samples were synthesized hydrothermally using H3BO3, H3PO4 and short chain n-alkylamines (n = 3, 4) as starting materials. The resulting products were characterized by powder X-ray diffraction (XRD), Fourier transform
infrared spectroscopy (FT-IR), scan electron microscopy (SEM) and transmission electron microscopy (TEM), respectively. A
possible mechanism for the formation of the materials is also discussed. |
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| Keywords: | Nano-sized BPO4 Core-shell BPO4 n-Alkylamine Hydrothermal synthesis |
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