| 反相悬浮法红薯淀粉/丙烯酸接枝反应工艺研究 |
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| 引用本文： | 申艳敏,赵培侠,朱春山.反相悬浮法红薯淀粉/丙烯酸接枝反应工艺研究[J].粮食与油脂,2012(4):23-25. |
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| 作者姓名： | 申艳敏 赵培侠 朱春山 |
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| 作者单位： | 河南工业大学化学化工学院,河南郑州450001 |
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| 摘 要： | 采用反相悬浮法以淀粉接枝丙烯酸合成吸水性树脂;探讨单体与淀粉质量配比、交联剂、引发剂、油水体积比、单体中和度等因素对树脂吸水率影响,通过单因素和正交实验得到最优工艺条件:单体与淀粉质量配比5∶1、交联剂用量0.122 g、引发剂用量1.3 g、油水体积比1.3∶1、单体中和度70%;聚合物在自来水中最大吸液倍率为95 g/g,且产品具有良好吸水速率。
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| 关 键 词： | 红薯淀粉 丙烯酸 反相悬浮 |
Graft co-polymerization of acrylic acid onto sweet potato starch in inverse suspension |
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| SHEN Yan-min,ZHAO Pei-xia,ZHU Chun-shan.Graft co-polymerization of acrylic acid onto sweet potato starch in inverse suspension[J].Cereals & Oils,2012(4):23-25. |
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| Authors: | SHEN Yan-min ZHAO Pei-xia ZHU Chun-shan |
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| Affiliation: | (School of Chemistry and Chemical Engineering,Henan University of Technology,Zhengzhou 450001,Henan,China) |
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| Abstract: | The effects of weight ratio of acrylic acid to starch,cross-linking agent,initiator agent,ratio of oil to water and neutralization content of monomer on reaction of graft co-polymerization of to water 1.3∶1,neutralization content of monomer 70%.Under the best polymerization condition,the acrylic acid onto starch in inverse suspension system were conducted.By single factor experiment and orthogonal experiment the optimum conditions were determined as weight ratio of acrylic acid to starch 5∶1,concentrations of cross-linking agent 0.122 g,concentrations of initiator agent 1.3 g,ratio of oil water-absorbency of polymer is 95 g/g.Also,the product with excellent speed of water absorption |
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| Keywords: | sweet potato starch acrylic acid inverse suspension |
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