| 用糠醛合成糠偶姻醋酸酯 |
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| 引用本文： | 高大维,贾晋礼,华士英,张玉敏,顾强,石龙. 用糠醛合成糠偶姻醋酸酯[J]. 精细化工, 1998, 0(4) |
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| 作者姓名： | 高大维 贾晋礼 华士英 张玉敏 顾强 石龙 |
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| 作者单位： | 吉林大学化学系，白求恩医科大学预防医学院 |
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| 摘 要： | 以糠醛为原料，ＶＢ１为催化剂，利用偶姻缩合反应合成了糠偶姻，糠偶姻被醋酐酯化为糠偶姻醋酸酯。熔点７２～７３℃，收率８８％～９０％。通过元素分析、ＧＣ ＭＣ谱、ＩＲ谱、１ＨＮＭＲ谱对所合成的糠偶姻醋酸酯进行了全面分析表征，证实了它的分子结构式
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| 关 键 词： | 糠醛，糠偶姻，糠偶姻醋酸酯 |
Synthesis of Furoin Acetate with Furfural |
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| Gao Dawei,Jia Jinli,Hua Shiying,Zhang Yumin,Gu Qiang. Synthesis of Furoin Acetate with Furfural[J]. Fine Chemicals, 1998, 0(4) |
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| Authors: | Gao Dawei Jia Jinli Hua Shiying Zhang Yumin Gu Qiang |
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| Abstract: | Furoin was synthesized by acyloin condensation starting from furfural and VB 1 as a catalyst, and followed by esterification into furoin acetate with acetic anhydride in 88%～90% yield.The m.p.of the product was 72～73℃. Synthesized furoin acetate was characterized by elementary analysis, GC MC spectrum,IR spectrum and 1 HNMR.The molecular structural formula of furoin acetate was demonstrated. |
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| Keywords: | furfural furoin furoin acetate |
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