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气相色谱/质谱法测定化妆品中5种麝香类禁限用物质
引用本文:李懿睿,武晓剑,王东辉,王虎. 气相色谱/质谱法测定化妆品中5种麝香类禁限用物质[J]. 香料香精化妆品, 2013, 0(4): 24-25
作者姓名:李懿睿  武晓剑  王东辉  王虎
作者单位:1. 上海计量测试技术研究院,上海,201203
2. 国家香精香料化妆品质量监督检验中心,上海,200232
基金项目:本文工作受国家质检总局科技计划项目资助
摘    要:建立了气相色谱/质谱法同时测定化妆品中5种麝香类物质的方法。将样品用乙醇或乙酸乙酯提取后直接经GC/MS测定。结果显示,此方法简便、快速、灵敏。方法的线性范围为1~500μg/mL,回收率不低于90%,RSD〈5%。

关 键 词:气相色谱  质谱法  化妆品  麝香类  禁限用物质

Determination of Five Musks in Cosmetics by Gas Chromatography/Mass Spectrometry
LI Yirui , WU Xiaojian , WANG Donghui , WANG Hu. Determination of Five Musks in Cosmetics by Gas Chromatography/Mass Spectrometry[J]. Flavour Fragrance Cosmetics, 2013, 0(4): 24-25
Authors:LI Yirui    WU Xiaojian    WANG Donghui    WANG Hu
Affiliation:1(1.Shanghai Institute of Measurement and Testing Technology,Shanghai 201203,China;2.National Quality Supervision & Inspection Centre of Fragrance Flavor & Cosmetics,Shanghai 200232,China)
Abstract:A gas chromatography-mass spectrometry method(GC/MS) had been developed for the simultaneous determination of five nmsks in cosmetics. The samples were extracted by ethanol or ethyl acetate and determined by GC/MS directly. The re stilts indicated that the method was easier, faster and more sensitive by using mass spectrometry as detector. The linear range was 1-500 ug/ml, recoveries were not less than 90%, and RSD 〈5%.
Keywords:GC/MS  cosmetic  musks  prohibited and restricted substances
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