Poly(butylene terephthalate)/Clay Nanocomposites directly Prepared from Pristine Montmorillonite (MMT) |
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Authors: | Junfeng Xiao Yuan Hu Qingkong Kong Lei Song Zhengzhou Wang Zuyao Chen Weicheng Fan |
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Affiliation: | (1) State Key Lab. of Fire Science, University of Science and Technology of China, Hefei, 230026, Anhui, P.R. China;(2) Department of Chemistry, University of Science and Technology of China, Hefei, 230026, Anhui, P.R. China |
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Abstract: | Summary Poly(butylene terephthalate) (PBT)/clay nanocomposites have been prepared by melt intercalation method directly from pristine montmorillonite (MMT), using cetyl pyridinium chloride (CPC) as the polymer/clay reactive compatibilizer. The effect of the reactive compatibilizer (CPC) proportion relative to the clay on the structure and properties of the PBT/clay nanocomposites was studied by XRD, TEM, TGA and cone calorimeter. The results show that such appropriate proportion as 1 wt % CPC to 3 wt % MMT induces well-dispersed intercalated morphology and better thermal and flame retarded properties. At last the intercalation mechanism of the technology was discussed. |
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