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吗啉离子液体中纳米TiO2的制备及其光催化性能
引用本文:赵金花,王宇松,陈武华,赖飞.吗啉离子液体中纳米TiO2的制备及其光催化性能[J].过程工程学报,2015,15(1):159-163.
作者姓名:赵金花  王宇松  陈武华  赖飞
作者单位:工商银行福建龙岩岩城支行 6222081410000389178 龙岩学院化学与材料学院 龙岩学院化学与材料学院 龙岩学院化学与材料学院
基金项目:福建省教育厅资助项目(编号:JA13307)
摘    要:以自制N-甲基-N-硝基苯基吗啉盐酸盐离子液体为介质,以TiOCl2溶液为前驱体,利用低温水解法制备了金红石型纳米TiO2粉体. 结果表明,所制TiO2粒径为4.7 nm,将其用于光催化降解甲基橙,5 h内甲基橙降解率可达99.18%,说明其具有优良的光催化性能.

关 键 词:N-甲基吗啉  离子液体  二氧化钛  纳米粉体  光催化  甲基橙  
收稿时间:2014-9-25
修稿时间:2014-12-12

Preparation and Photocatalytic Properties of Nanometer TiO2 Powder in Morpholine Ionic Liquid
ZHAO Jin-hua,WANG Yu-song,CHEN Wu-hua,LAI Fei.Preparation and Photocatalytic Properties of Nanometer TiO2 Powder in Morpholine Ionic Liquid[J].Chinese Journal of Process Engineering,2015,15(1):159-163.
Authors:ZHAO Jin-hua  WANG Yu-song  CHEN Wu-hua  LAI Fei
Affiliation:College of Chemistry and Material Science, Longyan College College of Chemistry and Material Science, Longyan College College of Chemistry and Material Science, Longyan College College of Chemistry and Material Science, Longyan College
Abstract:The rutile nanometer TiO2 powder was prepared using self-made N-methy-N-nitrophenyl morpholine hydrochloride ionic liquid as the medium and TiOCl2 solution as the precursor by low temperature hydrolysis method. The results show that the prepared TiO2 particle size is 4.7 nm. The nanometer TiO2 was used in photocatalytic degradation of methyl orange. The results show that the degradation rate can reach 99.18% in 5 h, which shows that the prepared nanometer TiO2 has excellent photocatalytic performance.
Keywords:N-methyl morpholine  ionic liquid  titanium dioxide  nanometer powder  photocatalysis  methyl orange
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