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Calcium phosphate coatings prepared by aerosol-gel
Affiliation:1. Departemento F??sica Aplicada, Universidad Autónoma de Madrid, 28049 Madrid, Spain;2. Laboratoire des Matériaux et du Génie Physique, INPG, BP 46, 38402 Saint Martin d''Hères, France;3. Instituto de Ciencia de Materiales de Madrid, CSIC, 28049, Madrid, Spain;1. Department of Orthopaedics, Trauma and Reconstructive Surgery, University Medical Center RWTH Aachen, Germany;2. Biomedical Engineering Institute, Chiang Mai University, Thailand;3. Department of Mechanical Engineering, Faculty of Engineering, Chiang Mai University, Thailand;4. Department of Orthopaedic and Trauma Surgery, Academic Hospital of Bolzano (SABES-ASDAA), Teaching Hospital of the Paracelsus Medical University, 39100, Bolzano, Italy;5. Department of Trauma and Reconstructive Surgery, BG Hospital Bergmannstrost, Halle (Saale), Germany;1. Departamento de Física Aplicada and Instituto de Ciencia de Materiales Nicolás Cabrera, Universidad Autónoma de Madrid, 28049, Madrid, Spain;2. Mecwins S.L., Parque Científico de Madrid PTM, Plaza de la Encina 10-11, Tres Cantos, 28760, Madrid, Spain;3. Centro de Microanálisis de Materiales, Universidad Autónoma de Madrid, 28049, Madrid, Spain;1. School of Information and Electrical Engineering, Hunan University of Science and Technology, Xiangtan 411201, China;2. Department of Physics and Electronic Science, Hunan University of Science and Technology, Xiangtan 411201, China;3. College of Mechanical and Electrical Engineering, Hunan University of Science and Technology, Xiangtan 411201, China
Abstract:The aerosol-gel process has been assayed for the deposition of calcium phosphate (CaP) coatings. The deposition conditions have been preliminarily studied in order to obtain polycrystalline hydroxyapatite (HAP) coatings. The evolution of composition, structure and morphology was monitored by FTIR, XRD and SEM techniques as a function of the sintering temperature. HAP coatings deposited on TiAlV substrates were further characterized by Auger and indentation techniques in order to measure their quantitative composition and adhesive strength, respectively. The results corroborate the high quality of aerosol-gel derived HAP coatings.
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