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| 4-氟-3-苯氧基苯甲醛的气相色谱分析方法 | |
| 引用本文： | 张梅凤,方浩,杨朝晖,唐永军,王智. 4-氟-3-苯氧基苯甲醛的气相色谱分析方法[J]. 现代农药, 2007, 6(5): 26-27 |
| 作者姓名： | 张梅凤 方浩 杨朝晖 唐永军 王智 |
| 作者单位： | 1. 山东大学,济南,250014;山东省农药研究所,济南,250100 2. 山东大学,济南,250014 3. 山东省农药研究所,济南,250100 4. 莱阳农学院植物保护学院,山东青岛,266109 |
| 摘 要： | 采用气相色谱法对4-氟-3-苯氧基苯甲醛进行定量测定,选用氢火焰离子化检测器,6%OV–17填充柱,正二十烷为内标,气化室和检测器温度为210℃,柱温160℃。该方法简单、快速、准确、适用,标准偏差0.19,变异系数0.20%,平均回收率100.0%。 |
| 关 键 词： | 4-氟-3-苯氧基苯甲醛 气相色谱 分析 |
| 文章编号： | 1671-5284（2007）05-0026-02 |
| 收稿时间： | 2007-02-28 |
| 修稿时间： | 2007-03-23 |
Gas Chromatographic Analysis of 4-Fluoro-3-phenoxy Benzaldehyde |
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| ZHANG Mei-Feng,FANG Hao,YANG Zhao-Hui,TANG Yong-Jun,WANG Zhi. Gas Chromatographic Analysis of 4-Fluoro-3-phenoxy Benzaldehyde[J]. Modern Agrochemicals, 2007, 6(5): 26-27 | |
| Authors: | ZHANG Mei-Feng FANG Hao YANG Zhao-Hui TANG Yong-Jun WANG Zhi |
| Affiliation: | 1. Shandong University,Jinan 250014,China; 2. Shandong Pesticide Research Institute,Jinan 250100,China; 3. Plant Protection Institute of Laiyang Agricultural College,Shandong Qingdao 266109,China |
| Abstract: | A method for the determination of 4-fluoro-3-phenoxy benzaldehyde by GC was established, using 1 m×2 mm glass column packed with 6% OV-101/Chromsorb W HP, n-eicosane as the internal standard. The temperature of injection and detector was 210℃,column temperature was 160℃.The method is simple, rapid, accurate and practical. The standard deviation and variation coefficient were 0.19 and 0.20% respectively, and the average recovery was 100.0%. |
| Keywords: | 4-fluoro-3-phenoxy benzaldehyde gas chromatography analysis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |