| HPLC法测定N-羟基-N-(2-((1-(4-氯苯基)-1H-吡唑-3-基)氧)甲基)苯基氨基甲酸甲酯 |
| |
| 引用本文： | 孔晓红,王艳丽. HPLC法测定N-羟基-N-(2-((1-(4-氯苯基)-1H-吡唑-3-基)氧)甲基)苯基氨基甲酸甲酯[J]. 精细化工中间体, 2015, 45(2): 70-72 |
| |
| 作者姓名： | 孔晓红 王艳丽 |
| |
| 作者单位： | 湖南化工研究院国家农药创制工程技术研究中心,湖南长沙410014;农用化学品湖南省重点实验室,湖南长沙410014 |
| |
| 摘 要： | 采用Aglient Extend-C185μm 250 mm×4.6 mm色谱柱,流动相为甲醇-0.4%磷酸溶液(v∶v=75∶25),流速为1 m L/min,275 nm为检测波长,建立了测定N-羟基-N-(2-((1-(4-氯苯基)-1H-吡唑-3-基)氧)甲基)苯基氨基甲酸甲酯含量的高效液相色谱分析方法。在进样量为0.53~3.52μg的范围内线性关系良好(y=125679.4x+15010.4,r=0.9999),RSD 0.24%,回收率99.2%~100.4%,分析周期为15 min。方法快速、简便、准确,可用于N-羟基-N-(2-((1-(4-氯苯基)-1H-吡唑-3-基)氧)甲基)苯基氨基甲酸甲酯反应液及产品的质量控制。
|
| 关 键 词： | N-羟基-N-(2-((1-(4-氯苯基)-1H-吡唑-3-基)氧)甲基)苯基氨基甲酸甲酯 HPLC 测定 |
Determination of methyl 2-((1-(4-chlorophenyl)-1H-pyrazol-3-yloxy)methyl)phenyl(hydroxy)carbamate by HPLC |
| |
| KONG Xiao-hong,WANG Yan-li. Determination of methyl 2-((1-(4-chlorophenyl)-1H-pyrazol-3-yloxy)methyl)phenyl(hydroxy)carbamate by HPLC[J]. Fine Chemical Intermediates, 2015, 45(2): 70-72 |
| |
| Authors: | KONG Xiao-hong WANG Yan-li |
| |
| Affiliation: | KONG Xiao-hong;WANG Yan-li;Hunan Research Institute of Chemical Industry, National Engineering Research Center for Agrochemicals;Hunan Province Key Laboratory for Agrochemicals; |
| |
| Abstract: | |
| |
| Keywords: | methyl 2-((1-(4-chlorophenyl)-1H-pyrazol-3-yloxy)methyl)phenyl(hydroxy)carbamate |
| 本文献已被 CNKI 等数据库收录！ |
