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CuS nanostructures prepared by a hydrothermal method
Authors:Qing-Li Huang  Hu ChenYong Cai Zhang  Chang Le Wu
Affiliation:a Testing center, Yangzhou University, Yangzhou city, Jiangsu 225009, China
b Key Laboratory of Environmental Material and Environmental Engineering of Jiangsu Province, College of Chemistry and Chemical Engineering, Yangzhou University, Jiangsu 225002, China
Abstract:Without using any surfactant or template, novel CuS three-dimensional (3D) structures consisting of nanosheets were successfully synthesized via a convenient one-step hydrothermal approach. X-ray diffraction pattern showed that the as-prepared product was pure hexagonal phase CuS. Scanning electron microscopy and high-resolution transmission electron microscopy images revealed that the as-prepared product comprised 3D microspheres (about 1-3 μm in diameter), which were further constructed with randomly oriented, single-crystalline CuS nanosheets (about 20 nm in thickness). The UV-vis absorption spectrum of the as-synthesized CuS 3D microspheres displayed an optical absorption minimum near 672 nm. Besides, the thermal stability of the as-synthesized CuS 3D microspheres was also studied.
Keywords:Chalcogenides  Crystal growth  Copper sulfide  Microstructure
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