| 微晶化加工含钾页岩的实验研究 |
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| 引用本文： | 朱再胜,骆振福,杨玉芬,盖国胜,吕乐福,于晓东,王可,赵家博. 微晶化加工含钾页岩的实验研究[J]. 中国矿业大学学报, 2012, 0(2): 293-298 |
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| 作者姓名： | 朱再胜 骆振福 杨玉芬 盖国胜 吕乐福 于晓东 王可 赵家博 |
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| 作者单位： | 中国矿业大学化工学院;浙江清华长三角研究院长兴粉体及新材料工程中心;清华大学材料科学与工程系;山东农业大学资源与环境学院 |
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| 基金项目： | 国家自然科学基金项目(50974079,51072097);科技部农业科技成果转化资金项目(2010GB23600657);国家自然科学基金委员会创新研究群体科学基金项目(50921002);中央高校基本科研业务费专项资金项目(2010ZDP01A06) |
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| 摘 要： | 采用自行研制的设备WJH-1微晶化加工含钾页岩,对产品进行分时段采样,运用激光粒度分析仪、比表面积仪、SEM和XRD对其粒度分布、比表面积、形貌、成分和晶体结构进行了表征,利用等球直径分析了物料d50,d97等粒度分布的变化及图表法分析比表面积和晶格参数的变化.结果表明:d50,d97随时间呈指数下降,在前1.5h减小幅度最大,d50下降幅度达到80.07%,d97下降幅度为79.68%;比表面积先增加后降低,然后又缓慢增加;选用四次多项式对比表面积与能耗的关系进行拟合,拟合效果良好;矿物晶体发生晶格畸变,结晶度降低,加工过程具有微晶化效果.
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| 关 键 词： | WJH-1 微晶化加工 含钾页岩 |
Experimental research on microcrystalling processing of potassic shale |
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| ZHU Zai-sheng,LUO Zhen-fu,YANG Yu-fen,GAI Guo-sheng,LV Le-fu,YU Xiao-dong,WANG Ke,ZHAO Jia-bo. Experimental research on microcrystalling processing of potassic shale[J]. Journal of China University of Mining & Technology, 2012, 0(2): 293-298 |
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| Authors: | ZHU Zai-sheng LUO Zhen-fu YANG Yu-fen GAI Guo-sheng LV Le-fu YU Xiao-dong WANG Ke ZHAO Jia-bo |
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| Affiliation: | 1(1.School of Chemical Engineering and Technology,China University of Mining & Technology,Xuzhou,Jiangsu 221116,China;2.Department of Materials Science and Engineering,Tsinghua University,Beijing 100084,China; 3.Changxing Powder and New Materials Engineering Center,Yangtze Delta Region Institute of Tsinghua University,Changxing,Zhejiang 313100,China;4.College of Resources and Environment, Shandong Agricultural University,Taian,Shandong 271018,China) |
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| Abstract: | The potassic shale was microcrystally processed by a WJH-1.The characteristics of samples at different processing time were characterized by a laser size distribution apparatus,specific surface area instrument,SEM and XRD.The changes of particle size distribution,including d50 and d97,and the changes of specific surface area and crystal lattice were analyzed.The results show that the exponential decrease of d50 and d97 with time is achieved.The extent of decrease in the prior 1.5 h is max,the d50 decreased by 80.07% and d97 79.68%.The specific surface area increases firstly,decreases soon after and then increases slowly.A better fitting between specific surface area and energy consumption was completed using a quartic polynomial.The lattice distortion occurred,the degree of crystallization is reduced and microcrystalling processing has been take place. |
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| Keywords: | WJH-1 microcrystallizing processing potassic shale |
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