氯苯硝化产物的检测

以Lewis酸作催化剂、硝酸作硝化剂进行氯苯硝化，主要产物是对硝基氯苯、邻硝基氯苯。对其硝化产物进行了定性分析，发现几乎不含间位及其他副产物。以硝基苯为内标物，采用多点校正作出了氯苯、对硝基氯苯、邻硝基氯苯的内标曲线，并对其准确度进行了验证，为氯苯硝化的研究找到一种简便、快捷的定量分析方法。

Detection for nitrified products of chlorobenzene

The main nitrified products of ehlorobenzene are p-mononitrochlorobenzen and o-mononitrochlorobenzen using Lewis acid as catalyst and nitric acid as nitrating agent. The nitrified products are qualitative analyzed, and find that there is no any other by- products at meta-position. The internal calibration curves of chlorobenzene, p-mononitrochlorobenzen and o-mononitrochlorobenzen are described through a few calibration points using nitrobenzene as internal calibration product, and the degree of accuracy is verified. A sort of simple and convenient quantitative method to research chlorobenzene nitration is seeked out.