| CCD-ICP-AES同时测定土壤中多种元素和校正基体干扰方法的研究 |
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| 引用本文： | 孙福生.CCD-ICP-AES同时测定土壤中多种元素和校正基体干扰方法的研究[J].苏州科技学院学报(工程技术版),1997(3). |
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| 作者姓名： | 孙福生 |
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| 作者单位： | 苏州城建环保学院科技处 |
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| 摘 要： | 文章研究了用电荷－耦合装置电感耦合等离子体发射光谱同时测定土壤中多种元素，并对校正基体干扰效应的方法进行了研究和比较。通过对欧共体参考局CRM143土壤标准参考物的测定，研究比较了基体匹配、单点标准加入和优化等离子体操作条件三种校正基体干扰效应的方法。其中单点标准加入法是最有效、经济和简单易操作的方法，并应用此法成功地测定了英国某工业区的土壤样品。
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| 关 键 词： | 电荷-耦合装置 电感耦合等离子体 原子发射光谱 校正基体效应 土壤 多元素同时测定 |
STUDY OF SIMULTANEOUS DETERMINATION OF MULTI-ELEMENT IN SOIL BY ICP-AES WITH A CCD AND METHOD FOR CORRECTION OF MATRIX INTERFERENCE EFFECT |
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| Sun Fusheng.STUDY OF SIMULTANEOUS DETERMINATION OF MULTI-ELEMENT IN SOIL BY ICP-AES WITH A CCD AND METHOD FOR CORRECTION OF MATRIX INTERFERENCE EFFECT[J].Journal of University of Science and Technology of Suzhou：Engineering and Technology,1997(3). |
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| Authors: | Sun Fusheng |
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| Affiliation: | Dept. of Science and Technology |
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| Abstract: | The simultaneous determination of multi-element in soil by ICP-AES with a CCD and the method for correction of matrix interference effect are studied and compared. Through the determination of CRM 143 soil standard reference material of Bureau Communautaire de Reference, we examine the following correction methods: matrix matching, single-point standard addition and optimisation of plasma operating conditions. Of them, the single- point standard addition method proves the most effective, economical and operational, and it has been successfully applied to determine the soil samples taken in a certain industrial area of the UK. |
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| Keywords: | CCD ICP AES correction of matrix effect soil simultaneous determination of multi-element |
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