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Specimen preparation for high-resolution transmission electron microscopy using focused ion beam and Ar ion milling
Authors:Sasaki Hirokazu  Matsuda Takeyoshi  Kato Takeharu  Muroga Takemi  Iijima Yasuhiro  Saitoh Takashi  Iwase Fusako  Yamada Yutaka  Izumi Teruo  Shiohara Yuh  Hirayama Tsukasa
Abstract:We have developed a focused ion beam (FIB)-Ar ion-milling technique for high-resolution transmission electron microscopy. A micrometresized specimen was mounted on a cross section of metal foil of a few micrometres thick, using FIB microsampling. Following this, a 2 degrees wedgeshaped part was made in the specimen using FIB. Finally, the specimen was milled using an Ar ion beam to remove the FIB-damaged layers. We applied the FIB-Ar ion milling technique to a CeO(2)/Gd(2)Zr(2)O(7) multilayer specimen, resulting in the crystal lattice fringes of both layers being clearly observable in comparison to a specimen finished using a Ga ion beam at an accelerating voltage of 10 kV.
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