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基于顶空气相离子迁移谱的干腐病马铃薯挥发性成分分析
引用本文:张凡,张宇帆,苏心悦,徐文雅,安焕炯,马倩云,孙剑锋,王颉,王文秀. 基于顶空气相离子迁移谱的干腐病马铃薯挥发性成分分析[J]. 食品科学, 2022, 43(6): 317-323. DOI: 10.7506/spkx1002-6630-20210403-039
作者姓名:张凡  张宇帆  苏心悦  徐文雅  安焕炯  马倩云  孙剑锋  王颉  王文秀
作者单位:(河北农业大学食品科技学院,河北保定 071000)
基金项目:河北省高等学校青年基金项目(QN2019113);河北省自然科学基金项目(C2020204166);河北省重点研发计划项目(20327111D;20327103D);河北农业大学引进人才科研专项(YJ201850)
摘    要:以健康和不同腐败程度(轻度干腐病、中度干腐病、重度干腐病)马铃薯样品为研究对象,基于顶空气相离子迁移谱(headspace-gas chromatography-ion mobility spectrometry,HS-GC-IMS)技术对不同病害程度马铃薯中挥发性成分进行鉴别分析.结果表明,不同腐败程度的马铃薯共检测...

关 键 词:马铃薯  干腐病  顶空气相离子迁移色谱  主成分分析  指纹图谱

Analysis of Volatile Components in Potatoes with Dry Rot by Headspace-Gas Chromatography-Ion Mobility Spectrometry
ZHANG Fan,ZHANG Yufan,SU Xinyue,XU Wenya,AN Huanjiong,MA Qianyun,SUN Jianfeng,WANG Jie,WANG Wenxiu. Analysis of Volatile Components in Potatoes with Dry Rot by Headspace-Gas Chromatography-Ion Mobility Spectrometry[J]. Food Science, 2022, 43(6): 317-323. DOI: 10.7506/spkx1002-6630-20210403-039
Authors:ZHANG Fan  ZHANG Yufan  SU Xinyue  XU Wenya  AN Huanjiong  MA Qianyun  SUN Jianfeng  WANG Jie  WANG Wenxiu
Affiliation:(College of Food Science and Technology, Hebei Agricultural University, Baoding 071000, China)
Abstract:In this study, headspace-gas chromatography-ion mobility spectrometry (HS-GC-IMS) was employed for the analysis of volatile substances in healthy potatoes and those with different degrees of dry rot (light, moderate and heavy). The results showed that 43 volatile components were identified, including 18 aldehydes, 9 alcohols, 5 ketones, 5 alkenes, 2 esters, 2 amines, 1 furan and 1 ether. The contents of octene, α-carcelene, cyclohexanone, heptyl aldehyde and acetaldehyde went up with increasing severity of dry rot, and dipropyl disulfide, styrene, isobutanol and nonenal were produced in samples with heavy soft rot as the specific volatile components related to metabolites of Fusarium sambucinum. Fingerprints were developed that allowed to visually discern the differences in volatile components between samples with different degrees of rot severity. Principal component analysis (PCA) showed that the healthy and rotten potatoes could be effectively distinguished based on volatile components. We concluded that HS-GC-IMS allows visual comprehensive identification of the differences in volatile components between potatoes with different degrees of rot severity and effective identification of the specific volatile components of potatoes with dry rot, which can provide the theoretical basis for the diagnosis and identification of dry rot in potatoes based on odor sensing information.
Keywords:potato   dry rot   headspace-gas chromatography-ion mobility spectrometry   principal component analysis   fingerprint,
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