| 雾化共沉淀法制备Ce0.8Gd0.2O1.9纳米粉体 |
| |
| 引用本文： | 杨建平,陈志刚,李霞章,陈杨. 雾化共沉淀法制备Ce0.8Gd0.2O1.9纳米粉体[J]. 电子元件与材料, 2007, 26(2): 17-19 |
| |
| 作者姓名： | 杨建平 陈志刚 李霞章 陈杨 |
| |
| 作者单位： | 江苏工业学院材料科学与工程系,江苏,常州,213016;江苏大学材料科学与工程学院,江苏,镇江,212013 |
| |
| 基金项目： | 江苏省自然科学基金 , 江苏省高新技术项目 |
| |
| 摘 要： | 采用雾化加料的方式,以碳酸氢铵为沉淀剂,制备了纳米Ce0.8Gd0.2O1.9粉体。探寻了制备过程中影响粉体颗粒大小及团聚的工艺参数,并对影响机理进行了探讨。结果表明:将沉淀剂雾化加入的工艺有利于得到分散性好、尺寸均匀的纳米粉体。在最佳工艺参数点,即(Ce3++Gd3+)浓度为0.2 mol/L,反应温度为60℃,r[AHC∶(Ce3++Gd3+)]为3∶1,制得的纳米Ce0.8Gd0.2O1.9颗粒粒径在15 nm左右。
|
| 关 键 词： | 无机非金属材料 纳米 CeO2基电解质材料 共沉淀 雾化 |
| 文章编号： | 1001-2028（2007）02-0017-03 |
| 修稿时间： | 2006-09-09 |
Preparation of nano-sized Ce0.8Gd0.2O1.9 powders by atomization co-deposition method |
| |
| YANG Jian-ping,CHEN Zhi-gang,LI Xia-zhang,CHEN Yang. Preparation of nano-sized Ce0.8Gd0.2O1.9 powders by atomization co-deposition method[J]. Electronic Components & Materials, 2007, 26(2): 17-19 |
| |
| Authors: | YANG Jian-ping CHEN Zhi-gang LI Xia-zhang CHEN Yang |
| |
| Affiliation: | 1. Department of Material Science and Engineering,Jiangsu Polytechnic University, Changzhou 213016, China; 2. School of Material Science and Engineering, Jiangsu University, Zhenjiang 212013, China |
| |
| Abstract: | Nano-sized Ce0.8Gd0.2O1.9(20 GDC) powders were prepared by atomization co-deposition method using ammonium hydrogen carbonate(AHC) as the precipitant.The process parameters which influenced the sizes and agglomeration of 20 GDC powers were studied and its influence mechanism was discussed.The results show that the method can gain small and homogeneous nano-sized powders.The optimum parameter for preparing 20 GDC are obtained,viz the molar concentration of(Ce3++ Gd3+) is 0.2 mol/L,the reaction temperature is 60 ℃,the molar ratio of AHC and(Ce3++ Gd3+) is 3.Under such conditions the 15 nm 20 GDC powders are obtained. |
| |
| Keywords: | non-metallic inorganic material nanometer ceria-based electrolytes co-deposition atomization |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
