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球磨时间对粉末冶金制备Ti35Nb2.5Sn/10HA生物复合材料微观组织的影响(英文)
引用本文:王晓鹏,徐丽娟,陈玉勇,禹基道,肖树龙,孔凡涛,刘志光.球磨时间对粉末冶金制备Ti35Nb2.5Sn/10HA生物复合材料微观组织的影响(英文)[J].中国有色金属学会会刊,2012,22(3):608-612.
作者姓名:王晓鹏  徐丽娟  陈玉勇  禹基道  肖树龙  孔凡涛  刘志光
作者单位:哈尔滨工业大学材料科学与工程学院;哈尔滨工业大学金属精密热加工国家重点实验室;全北国立大学先进材料工程研究部
基金项目:Project(ZJY0605-02) supported by the Natural Science Foundation of Heilongjiang Province,China;Project(310703002) supported by the National Research Foundation of Korea(NRF) grant funded Korea Government
摘    要:采用高能机械球磨和脉冲电流活化烧结方法制备了一种新型的β-钛合金基体的Ti35Nb2.5Sn/10HA生物复合材料。研究了机械球磨不同时间的Ti35Nb2.5Sn10HA粉体以及烧结样品的微观组织。结果表明:经机械球磨8h后,粉体中的α-钛开始向β-钛转化。当球磨时间达到12h时,球磨粉体中的α-钛相完全转化为β-钛相,而且得到超细尺寸的复合粉体。用球磨12h的粉末烧结制备的复合材料具有超细晶粒结构,烧结得到的复合材料的硬度和相对密度都随着球磨时间的延长而增加。

关 键 词:Ti35Nb2.5Sn/10HA  超细晶粒  粉末冶金  球磨时间
收稿时间:9 September 2011

Effect of milling time on microstructure of Ti35Nb2.5Sn/10HA biocomposite fabricated by powder metallurgy and sintering
WANG Xiao-peng,XU Li-juan,CHEN Yu-yong,KEE Do-Woo,XIAO Shu-long,KONG Fan-tao,LIU Zhi-guang.Effect of milling time on microstructure of Ti35Nb2.5Sn/10HA biocomposite fabricated by powder metallurgy and sintering[J].Transactions of Nonferrous Metals Society of China,2012,22(3):608-612.
Authors:WANG Xiao-peng  XU Li-juan  CHEN Yu-yong  KEE Do-Woo  XIAO Shu-long  KONG Fan-tao  LIU Zhi-guang
Affiliation:1,2 1.School of Materials Science and Engineering,Harbin Institute of Technology,Harbin 150001,China;2.National Key Laboratory for Precision Hot Processing of Metals,Harbin Institute of Technology,Harbin 150001,China;3.Division of Advanced Material Engineering and Research Center of Advanced Materials Technology,Chonbuk National University,Chonbuk 561-756,Korea
Abstract:A new β-Ti based Ti35Nb2.5Sn/10 hydroxyapitite(HA) biocompatible composite was fabricated by mechanical milling and pulsed current activated sintering(PCAS).The microstructures of Ti35Nb2.5Sn/10HA powder particles and composites sintered from the milled powders were studied.Results indicated that α-Ti phase began to transform into β-Ti phase after the powders were mechanically milled for 8 h.After mechanical milling for 12 h,α-Ti completely transformed into β-Ti phase,and the ultra fine Ti35Nb2.5Sn/10HA composite powders were obtained.And ultra fine grain sized Ti35Nb2.5Sn/10HA sintered composites were obtained by PCAS.The hardness and relative density of the sintered composites both increased with increasing the ball milling time.
Keywords:Ti35Nb2  5Sn/10HA  ultrafine grain  powder metallurgy  milling time
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