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3-氯-2-丙烯基苯醚的合成
引用本文:张大洋,张显强,高宏开,赵鸣玉.3-氯-2-丙烯基苯醚的合成[J].沈阳化工学院学报,1995(3).
作者姓名:张大洋  张显强  高宏开  赵鸣玉
作者单位:沈阳化工学院精细化工系
摘    要:用D,D-混剂为原料制备了标题化合物。实验考察了催化剂种类及用量、反应温度、时间、物料配比等因素对反应转化率的影响。应用逐步回归分析方法处理数据,给出了定量描述反应条件与转化率相关关系的经验方程。在所确定的反应条件下,反应转化率大于90%。

关 键 词:相转移催化剂  亲核取代  烷基化  逐步回归

Synthesis of 3-Chloro-2-Propenyl Phenyl Ethers
Zhang Dayang, Zhang Xianqiang, Gao Hongkai, Zhao Mingyu.Synthesis of 3-Chloro-2-Propenyl Phenyl Ethers[J].Journal of Shenyang Institute of Chemical Technolgy,1995(3).
Authors:Zhang Dayang  Zhang Xianqiang  Gao Hongkai  Zhao Mingyu
Abstract:The title compounds were prepared with the D,D-mixture. The influence of cata-lysts, temperature,time and ratio of raw materials on the conversion was investigated.By using the stepwise regression,the experimental data were treated and the regression equations, which quantitatively describe the relation between the reaction conditions andthe conversion,were obtained,At the given suitable reaction conditions,the reaction conversion was more than 9 0 percent.
Keywords:hase transfer catalyst  nucleophilic subetitution  alkylation  step-wise regression
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