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2,4-二氯甲苯生产工艺的改进
引用本文:李波,袁志明,吴英. 2,4-二氯甲苯生产工艺的改进[J]. 精细化工中间体, 2004, 34(2): 62-64
作者姓名:李波  袁志明  吴英
作者单位:株洲化工集团有限责任公司,湖南,株洲,412004;株洲化工集团有限责任公司,湖南,株洲,412004;株洲化工集团有限责任公司,湖南,株洲,412004
摘    要:针对目前国内2,4 二氯甲苯生产工艺存在的主要问题,通过改进氯化合成工艺,采用先进碱洗精馏技术,提高了氯化反应收率和碱洗精馏效果,其中氯化反应收率达到了75%以上,氯气利用率>92%,产品质量在99.5%以上,从而有效地降低了生产成本,减少了环境污染,经济效益和社会效益显著,具有很好的推广应用前景。

关 键 词:2  4-二氯甲苯  生产工艺  改进  氯化  精馏
文章编号:1009-9212(2004)04-0062-03
修稿时间:2004-02-18

Improvement on the Synthesis Process of 2,4-Dichlorotoluene
LI Bo,YUAN Zhi-ming,WU Ying. Improvement on the Synthesis Process of 2,4-Dichlorotoluene[J]. Fine Chemical Intermediates, 2004, 34(2): 62-64
Authors:LI Bo  YUAN Zhi-ming  WU Ying
Abstract:Against the defects of current domestic synthesis process of 2,4-dichlorotoluene, improvement have been made by applying advanced alkaline rectification technologies. Consequently,The reaction yield is raised and rectification effect is bettered-reaction yield of chlorine is now over 75%;Utilization ratio of chlorine exceeds 92% and product qualification exceeds 99.5%. Therefore, production cost is cut down and pollution is minimized. All this indicates that the improvement is of remarkable economic and social benefits with prospects of being applied extensively.
Keywords:2  4-dichlorotoluene  synthesis process  improvement  chloration  rectification
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