| 苯并三嗪酮-3-胺衍生物的合成与杀虫活性研究 |
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| 引用本文： | 左金江,任叶果,柳爱平,裴晖,白建军,黄路,韩魁元,余一平,尹笃林.苯并三嗪酮-3-胺衍生物的合成与杀虫活性研究[J].精细化工中间体,2013(2):9-12. |
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| 作者姓名： | 左金江 任叶果 柳爱平 裴晖 白建军 黄路 韩魁元 余一平 尹笃林 |
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| 作者单位： | 湖南师范大学化学化工学院;湖南化工研究院国家农药创制工程技术研究中心;农用化学品湖南省重点实验室;长沙理工大学化学与生物工程学院 |
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| 基金项目： | 国家重点基础研究发展计划(973)项目(2010CB126104);国家自然科学基金资助项目(21272062);“十二五”国家科技支撑计划课题(2011BAE06B01);湖南省自然科学基金资助项目(11JJ2006,11FF3022) |
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| 摘 要： | 设计并合成了10个苯并三嗪酮-3-胺类化合物,其化学结构经1H NMR和MS分析确证。初步生物活性测试表明:该类化合物具有杀虫活性,如在500 mg/L浓度下,化合物4c、4d和7c对粘虫(Mythimna separate)的活性达到80%以上;在500 mg/L浓度下,化合物7d对蚜虫(Aphis fabae)的活性达到80%以上,对螨虫棉红蜘蛛(Tetranchus urticae)的活性达到70%以上。
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| 关 键 词： | 苯并三嗪酮-3-胺 合成 杀虫活性 |
Synthesis and Insecticidal Activity of Benzotriazinone-3-amine Derivatives |
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| ZUO Jin-jiang,REN Ye-guo,LIU Ai-ping,PEI Hui,BAI Jian-jun,HUANG Lu,HAN Kui-yuan,YU Yi-ping,YIN Du-lin.Synthesis and Insecticidal Activity of Benzotriazinone-3-amine Derivatives[J].Fine Chemical Intermediates,2013(2):9-12. |
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| Authors: | ZUO Jin-jiang REN Ye-guo LIU Ai-ping PEI Hui BAI Jian-jun HUANG Lu HAN Kui-yuan YU Yi-ping YIN Du-lin |
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| Affiliation: | 1(1.College of Chemistry and Chemical Engineering,Hunan Normal University,Changsha 410081,China;2.National Engineering Research Center for Agrochemicals,Hunan Research Institute of Chemical Industry,Changsha 410014,China;3.Hunan Province Key Laboratory for Agrochemicals,Changsha 410014,China) |
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| Abstract: | Ten novel benzotriazinone-3-anime derivatives were designed and synthesized,and their structures were confirmed by 1H NMR and MS spectra.The preliminary bioassay results showed that the title compounds possessed insecticidal activity.At the concentration of 500 mg / L,compands 4c,4d and 7c showed more than 80% insecticidal activities against Mythimna separata;at 500 mg / L,compand 7d showed more than 80 % insecticidal activity against Aphis fabae and more than 70% insecticidal activity against Tetranchus urticae. |
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| Keywords: | benzotriazinone synthesis insecticidal activities |
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