The Synthesis and Evaluation of Up-scalable Molybdenum Based Ultra Dispersed Catalysts: Effect of Temperature on Particle Size |
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Authors: | John Thompson Alejandro Vasquez Josephine M. Hill Pedro Pereira-Almao |
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Affiliation: | 1. Schulich School of Engineering, Department of Chemical and Petroleum Engineering, University of Calgary, Calgary, Alberta, Canada, T2N 1N4
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Abstract: | Unsupported molybdenum (Mo) micro/nanoparticle size range catalysts have been synthesized via precursor salts dissolved within a water-in-oil emulsion and online injected to a decomposition zone simulating processing conditions. The particles were characterized via DLS, reactivity tests and SEM. The effect of decomposition temperature on particle sizes was studied in both a horizontal reactor and vertical reactor configuration. |
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