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The Synthesis and Evaluation of Up-scalable Molybdenum Based Ultra Dispersed Catalysts: Effect of Temperature on Particle Size
Authors:John Thompson  Alejandro Vasquez  Josephine M. Hill  Pedro Pereira-Almao
Affiliation:1. Schulich School of Engineering, Department of Chemical and Petroleum Engineering, University of Calgary, Calgary, Alberta, Canada, T2N 1N4
Abstract:Unsupported molybdenum (Mo) micro/nanoparticle size range catalysts have been synthesized via precursor salts dissolved within a water-in-oil emulsion and online injected to a decomposition zone simulating processing conditions. The particles were characterized via DLS, reactivity tests and SEM. The effect of decomposition temperature on particle sizes was studied in both a horizontal reactor and vertical reactor configuration.
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