| 固体超强碱催化合成蔗糖硬脂酸酯 |
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| 引用本文： | 周建平,李先红,刘榛榛.固体超强碱催化合成蔗糖硬脂酸酯[J].应用化工,2005,34(7):452-454. |
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| 作者姓名： | 周建平 李先红 刘榛榛 |
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| 作者单位： | 襄樊学院,化学与生物科学系,湖北,襄樊,441053 |
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| 摘 要： | 利用固体超强碱催化剂合成蔗糖硬脂酸酯,考察了反应时间、反应温度、原料配比以及催化剂用量对蔗糖硬脂酸酯产率的影响,得出最佳合成条件为：硬脂酸甲酯：蔗糖(摩尔比)=2∶1；催化剂用量为原料总量的6％；反应时间8 h；反应温度130～140℃。
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| 关 键 词： | 固体超强碱 蔗糖酯 合成 |
| 文章编号： | 1671-3206(2005)07-0452-03 |
| 修稿时间： | 2005年5月19日 |
Synthesis of sucrose stearate by solid superbase catalyst |
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| ZHOU Jian-ping,LI Xian-hong,LIU Zhen-zhen.Synthesis of sucrose stearate by solid superbase catalyst[J].Applied chemical industry,2005,34(7):452-454. |
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| Authors: | ZHOU Jian-ping LI Xian-hong LIU Zhen-zhen |
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| Affiliation: | ZHOU Jian-ping,L1 Xian-hong,LIU Zhen-zhen |
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| Abstract: | Using sucrose and methylstearate as the materials, sucrose stearate is synthesized with solid superbase catalyst, the factors of reaction time, reaction temperature, mixture ratio and the dosage of catalysteffect on the yield of sucrose stearate were studied. The optimal synthetic conditions are as foUows:themole ratio of methylstearate to sucrose is 2:1,the amount of catalyst is 6% of the reactants,the reactiontemperature is 120～130℃ ,and the reaction time is 8 h. |
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| Keywords: | solid superbase catalyst sucrose stearlate synthesis |
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