| 三苄基锡炔基膦酸酯的合成及波谱分析 |
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| 引用本文： | 尹汉东,张如芬,马春林.三苄基锡炔基膦酸酯的合成及波谱分析[J].化学世界,2000,22(2):78-79. |
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| 作者姓名： | 尹汉东 张如芬 马春林 |
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| 作者单位： | 聊城师范学院化学系,聊城 252059 |
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| 摘 要： | 合成了6个新的三苄基锡炔基膦酸酯(PhCH2)3Sn]2O2P(O)C≡CR(R≡n-C5H11,n-C6H13n-C7H15Ph,CH2OCH3,CH2OC2H5),对产物进行了红外光谱及核磁共振氢谱分析。
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| 关 键 词： | 三苄基锡 炔基膦酸酯 合成 生物活性 |
| 文章编号： | 0367-6358(2000)02-0075-03 |
Synthesis of tribenzyltin alkynylphosphates and analysis of their IR and 1HNMR spectra |
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| ZHANG Lin
GAO Wen-de ,XIAO Shu-xin ,XIE Ru-gang.Synthesis of tribenzyltin alkynylphosphates and analysis of their IR and 1HNMR spectra[J].Chemical World,2000,22(2):78-79. |
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| Authors: | ZHANG Lin
GAO Wen-de XIAO Shu-xin XIE Ru-gang |
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| Affiliation: | ZHANG Lin
(Institute of Nuclear Physics and Chemtstry,China Academy of Engineering Phyaics,Sichuan
Mianyang 621900)
GAO Wen-de ,XIAO Shu-xin ,XIE Ru-gang
(Chemistry Department of Sichuan University,Sichuan Chengdu 610064,China) |
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| Abstract: | A simple,efficient and novel
method for the synthesis of bromobenzene-d from commercial benzene-d(99.32D%) is
described.Fe and a little I were used as the catalysts,and the method of crude product
solution treatment was improved by solid K CO. The yield of bromobenzene-d was 72.5%,and
the deuterium content is about 99.2% measured by HNMR. |
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