| 三苄基锡炔基膦酸酯的合成及波谱分析 |
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| 引用本文： | 尹汉东,张如芬,马春林. 三苄基锡炔基膦酸酯的合成及波谱分析[J]. 化学世界, 2000, 22(2): 78-79 |
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| 作者姓名： | 尹汉东 张如芬 马春林 |
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| 作者单位： | 聊城师范学院化学系,聊城 252059 |
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| 摘 要： | 合成了6个新的三苄基锡炔基膦酸酯[(PhCH2)3Sn]2O2P(O)C≡CR(R≡n-C5H11,n-C6H13n-C7H15Ph,CH2OCH3,CH2OC2H5),对产物进行了红外光谱及核磁共振氢谱分析。
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| 关 键 词： | 三苄基锡 炔基膦酸酯 合成 生物活性 |
| 文章编号： | 0367-6358(2000)02-0075-03 |
Synthesis of tribenzyltin alkynylphosphates and analysis of their IR and 1HNMR spectra |
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| ZHANG Lin GAO Wen-de ,XIAO Shu-xin ,XIE Ru-gang. Synthesis of tribenzyltin alkynylphosphates and analysis of their IR and 1HNMR spectra[J]. Chemical World, 2000, 22(2): 78-79 |
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| Authors: | ZHANG Lin GAO Wen-de XIAO Shu-xin XIE Ru-gang |
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| Affiliation: | ZHANG Lin (Institute of Nuclear Physics and Chemtstry,China Academy of Engineering Phyaics,SichuanMianyang 621900)GAO Wen-de ,XIAO Shu-xin ,XIE Ru-gang (Chemistry Department of Sichuan University,Sichuan Chengdu 610064,China) |
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| Abstract: | A simple,efficient and novelmethod for the synthesis of bromobenzene-d from commercial benzene-d(99.32D%) isdescribed.Fe and a little I were used as the catalysts,and the method of crude productsolution treatment was improved by solid K CO. The yield of bromobenzene-d was 72.5%,andthe deuterium content is about 99.2% measured by HNMR. |
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