| 活性炭模板法制备锡酸锌掺杂磷化合物及表征 |
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| 引用本文： | 陈灵智,孙会娟,张明明,王玉,徐建中.活性炭模板法制备锡酸锌掺杂磷化合物及表征[J].化工新型材料,2021(3):156-158. |
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| 作者姓名： | 陈灵智 孙会娟 张明明 王玉 徐建中 |
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| 作者单位： | 衡水学院应用化学系;河北大学化学与环境科学学院 |
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| 基金项目： | 衡水学院校级课题(2020ZR11);河北省科技计划资助项目(17211414)。 |
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| 摘 要： | 选用磷酸活化后的活性炭为模板,NaSnO3·3H2O、ZnSO4·7H2O为原料,通过生物质模板法制备了锡酸锌掺杂磷(Zn2SnO4/P)化合物。通过X射线粉末衍射(XRD)、扫描电子显微镜(SEM)和N_2吸脱附等温线对制备的Zn2SnO4/P的结构、形貌进行表征。结果表明:Zn2SnO4/P为尖晶石结构,其形貌基本上和活性炭相匹配。其比表面积、孔体积和平均孔径分别为87m2/g、0.20cm3/g和9.0nm。
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| 关 键 词： | 活性炭 模板 锡酸锌掺杂磷 |
Preparation and characterization of zinc stannate doped with phosphorus compounds by activated carbon template |
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| Chen Lingzhi,Sun Huijuan,Zhang Mingming,Wang Yu,Xu Jianzhong.Preparation and characterization of zinc stannate doped with phosphorus compounds by activated carbon template[J].New Chemical Materials,2021(3):156-158. |
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| Authors: | Chen Lingzhi Sun Huijuan Zhang Mingming Wang Yu Xu Jianzhong |
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| Affiliation: | (Department of Applied Chemistry,Hengshui University,Hengshui 053000;College of Chemistry and Environmental Science,Hebei University,Baoding 071002) |
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| Abstract: | Zinc stannate doped with phosphorus was prepared by biomass template method with Phosphoric acid activated activated carbon as template,NaSnO3·3H2O and ZnSO4·7H2O as raw materials.The structure and morphology of Zn2SnO4/P were characterized by X-ray powder diffraction(XRD),scanning electron microscope(SEM)and Nitrogen adsorption desorption isotherm.The results showed that Zn2SnO4/P was spinel structure and morphology basically matches that of activated carbon.Specific surface area,pore volume and average pore diameter were 87m2/g,0.20cm3/g and 9.0nm,respectively. |
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| Keywords: | activated carbon template zinc stannate doped with phosphorus |
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