Conventional and microwave-assisted solvent-free synthesis of fused [1,2,5]thiadiazolo[3,4-b]quinoxaline-2,2-dioxide derivatives |
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Abstract: | A simple, highly efficient and environmentally friendly procedure for the condensation of $o$-phenylenediamine with 2,5-dialkyl-1,2,5-thiadiazolidine-3,4-dione-1,1-dioxides via two microwave-assisted reactions is described. These compounds were also prepared via a conventional heating method to provide a comparison with the microwave-assisted irradiation reaction protocol. The structures of the synthesized compounds were confirmed using infrared, 1H NMR and mass spectral analysis. |
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Keywords: | microwave cyclic sulfamides sulfur heterocycles thiadiazolidine quinoxaline |
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