Odor‐Free Lignin from Lignocellulose by Means of High Pressure Unit Operations: Process Design,Assessment and Validation |
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Authors: | Wienke Reynolds Victor Baudron Christian Kirsch Lisa M Schmidt Hannah Singer Lilia Zenker Carsten Zetzl Irina Smirnova |
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Affiliation: | 1. Hamburg University of Technology, Institute of Thermal Separation Processes, Eissendorfer Stra?e 38, 21073 Hamburg, Germany;2. Hamburg University of Technology, Institute of Environmental Technology and Energy Economics, Eissendorfer Stra?e 40, 21073 Hamburg, Germany. |
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Abstract: | In this work a process for the production of odor‐free lignin from wheat straw using solely water, enzymes and CO2 is described. Wheat straw pellets are pretreated by liquid hot water and enzymatic hydrolysis in a pilot plant with a capacity of 40 L, which enables the production of 3 – 4 kg of Aquasolv lignin per batch. Dried lignin samples are further treated using supercritical CO2, resulting into extraction of a large number of odorous free fatty acids and volatile organic compounds. All process steps can be sequentially conducted in a fixed‐bed via different sustainable solvents in a throughput regime. |
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Keywords: | Enzymatic hydrolysis Fixed‐bed Lignin Liquid hot water Pilot plant Supercritical fluid extraction |
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