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高灵敏度XRF对轻质燃油中硅含量的快速分析表征
引用本文:章然 吴梅 王杰明 刘明星. 高灵敏度XRF对轻质燃油中硅含量的快速分析表征[J]. 石油炼制与化工, 2006, 51(3): 89-93
作者姓名:章然 吴梅 王杰明 刘明星
作者单位:中国石化石油化工科学研究院
摘    要:建立利用高灵敏度能量色散X射线荧光光谱仪快速测定轻质燃油中硅含量的方法,并进行准确性和重复性考察。结果表明:该测定方法在硅质量分数为0~100 ug/g范围内的定量标准曲线具有良好的线性关系,R2大于0.999 9;方法检出限为1 μg/g,样品回收率为95.7%~103.0%,相对标准偏差小于5.79%,可用于汽油中硅含量的测定。

关 键 词:能量色散  X射线荧光光谱  汽油    
收稿时间:2019-09-05

FAST DETERMINATION OF SILICON CONTENT IN GASOLINE BY HF-XRF
Zhang Ran Wu Mei Wang Jieming Liu Mingxing. FAST DETERMINATION OF SILICON CONTENT IN GASOLINE BY HF-XRF[J]. Petroleum Processing and Petrochemicals, 2006, 51(3): 89-93
Authors:Zhang Ran Wu Mei Wang Jieming Liu Mingxing
Abstract:A method for fast determination of silicon content in gasoline by HF-XRF was developed. The precision of this method was inspected. The results showed that the linear correlation coefficient was more than 0.999 9 when the mass fraction of the silicon was 0-100 μg/g. The detection limit was 1μg/g for silicon,the standard addition recovery was in the range of 95.7%-103.0%,and the relative standard deviation was less than 5.79%. The results showed that this method is suitable for determination of silicon in gasoline.
Keywords:energy-dispersive   X-ray fluorescence  gasoline  silicon  
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