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电子鼻对花椒精油的辨别研究
引用本文:郑福平,宁洪良,郑景洲,谢建春,刘玉平,孙宝国.电子鼻对花椒精油的辨别研究[J].北京轻工业学院学报,2010(4):9-15.
作者姓名:郑福平  宁洪良  郑景洲  谢建春  刘玉平  孙宝国
作者单位:[1]北京工商大学化学与环境工程学院/食品添加剂与配料北京高校工程研究中心,北京100048 [2]北京天利海香精香料有限公司,北京101200 [3]Alpha M.O.S.公司亚太办事处,上海200336
基金项目:北京市教育委员会人才强教项目.
摘    要:以超临界流体萃取法和无溶剂微波萃取法提取了四川大红袍花椒和陕西韩城大红袍花椒精油,用电子鼻对花椒产地、提取方法和同种提取方法下的不同提取工艺条件下所得花椒精油进行了辨别研究.采用主成分分析法分析花椒精油的特征气味指纹图,发现电子鼻可以有效区分花椒精油.各主成分分析图中,第1、第2主成分累积方差贡献率为98.989%~99.5969%,辨别指数为93~95.初步探索了统计质量控制法控制花椒精油质量和判别因子分析法判断花椒精油的来源的可行性.

关 键 词:花椒  精油  电子鼻  主成分分析  辨别指数

USE OF AN ELECTRONIC NOSE TO DIFFERENTIATE ZANTHOXYLUM BUNGEANUM MAXIM. OILS
ZHENG Fu-ping,NING Hong-liang,ZHENG Jing-zhou,XIE Jian-chun,LIU Yu-ping,SUN Bao-guo.USE OF AN ELECTRONIC NOSE TO DIFFERENTIATE ZANTHOXYLUM BUNGEANUM MAXIM. OILS[J].Journal of Beijing Institute of Light Industry,2010(4):9-15.
Authors:ZHENG Fu-ping  NING Hong-liang  ZHENG Jing-zhou  XIE Jian-chun  LIU Yu-ping  SUN Bao-guo
Affiliation:1. College of Chemical and Environmental Engineering/Beijing Higher Institution Engineering Research Center of Food Additives and Ingredients, Beijing Technology and Business University, Beijing 100048, China ; 2. Beijing Tianlihai Flavor and Fragrance Co. ,Ltd, Beijing 101200, China; 3. Alpha M. O. S. , Asia Pacific Representative Office, Shanghai 200336, China)
Abstract:Essential oils were extracted from Zanthoxylum bungeanum Maxim. in Sichuan Province and in Hancheng City, Shaanxi Province by supercritical fluid extraction and solvent-free microwave extraction respectively. The electronic nose was used to discriminate the essential oils extracted from various origin of Zanthoxylum bungeanum Maxim. , and by using different extraction method and process conditions. The odor fingerprint of the essential oils was analyzed by principal component analysis method. It shows that the essential oils of Zanthoxylum bungeanum Maxim. can be differentiated by electronic nose. The accumulated variance contribution rates of principal component 1 and 2 are among 98. 989% 99. 5969% with discrimination index among 93 - 95 in each PCA charts. The feasibility of using statisti- cal quality control method in quality control and using discriminant factorial analysis method to discriminate the oils was studied preliminarily.
Keywords:Zanthoxylum bungeanum Maxim    essential oil  electronic nose  principal component analysis  discrimination index
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