| 苯甲醇制备苯甲酸的实验研究 |
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| 引用本文： | 李敏,陈志敏,程喜英.苯甲醇制备苯甲酸的实验研究[J].兵工学报,2007,28(6):758-760. |
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| 作者姓名： | 李敏 陈志敏 程喜英 |
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| 作者单位： | 太原工业学院,山西,太原,030008;太原工业学院,山西,太原,030008;太原工业学院,山西,太原,030008 |
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| 摘 要： | 制备了十六烷基三甲基磷钨杂多酸铵，并用其作为催化剂催化过氧化氢氧化苯甲醇制苯甲酸，分析了反应温度、反应时间、过氧化氢用量、催化剂用量对苯甲酸产率的影响。结果表明苯甲酸产率可达到86.3%．
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| 关 键 词： | 分析化学 十六烷基三甲基磷钨杂多酸铵 苯甲醇 过氧化氢 苯甲酸 |
| 文章编号： | 1000-1093（2007）06-0758-03 |
| 修稿时间： | 2006-01-26 |
Study of the Best Technological Condition for Preparating Phenyl Carboxylic Acid with Phenyl Methanol |
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| LI Min,CHEN Zhi-min,CHENG Xi-ying.Study of the Best Technological Condition for Preparating Phenyl Carboxylic Acid with Phenyl Methanol[J].Acta Armamentarii,2007,28(6):758-760. |
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| Authors: | LI Min CHEN Zhi-min CHENG Xi-ying |
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| Affiliation: | Taiyuan Institute of Technology, Taiyuan 030008, Shanxi, China |
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| Abstract: | The phenyl carboxylic acid was prepared from the oxidized phenyl methanol by the calalyzed hydrogen peroxide with the amine hexadecane trimethyl PW heteropoly acid used as the catalyst. The influence of reaction temperature, reaction period, hydrogen peroxide content and catalyst content on the yield rate of phenyl carboxylic acid was investigated. The results show that the yield rate of phenyl carboxylic acid is up to 86.3 %. |
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| Keywords: | analytical chemistry amine hexadecane trimethyl PW heteropoly acid phonyl methanol hydrogen peroxide phenyl carboxylic acid |
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