| 己酸己酯的催化合成 |
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| 引用本文： | 何建英,刘素环,陈丹云. 己酸己酯的催化合成[J]. 化工中间体, 2007, 0(4): 7-8,34 |
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| 作者姓名： | 何建英 刘素环 陈丹云 |
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| 作者单位： | 1. 河南大学,化学化工学院,河南,开封,475001
2. 商丘职业技术学院,农学系,河南,商丘,47600 |
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| 基金项目： | 河南省教育厅自然科学基金 , 河南省教育厅自然科学基金 |
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| 摘 要： | 采用硫酸氢钠为催化剂合成了己酸己酯，考察了催化剂用量、醇酸物质的量比、反应时间、带水剂用量及催化剂重复使用次数等因素对收率的影响。结果表明该催化剂具有催化活性高，易分离回收，操作简单，后处理方便，重复使用性良好等优势。最佳反应条件下收率为98．6％。
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| 关 键 词： | 己酸己酯 硫酸氢钠 催化 合成 |
| 文章编号： | 1006-253x（2007）04-007-2 |
| 收稿时间： | 2006-12-28 |
| 修稿时间： | 2006-12-28 |
Synthesis of Hexyl Hexanoate Catalyzed by Sodium Bisulfate |
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| HE Jian-ying,LIU Su-huan,CHEN Dan-yun. Synthesis of Hexyl Hexanoate Catalyzed by Sodium Bisulfate[J]. , 2007, 0(4): 7-8,34 |
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| Authors: | HE Jian-ying LIU Su-huan CHEN Dan-yun |
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| Affiliation: | HE Jian-ying,LIU Su-huan, CHEN Dan-yun (1.Chemistry and Chemical Engineering College of Henan University, Kaifeng 475001,Henan, China; 2. Shangqiu Vocational and Technical eollege,Shangqiu 476000,Henan, China) |
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| Abstract: | By using sodium bisulfate as the catalyst, hexyl hexanoate was synthesized. The investigated effects conclueded amount of the catalyst, reaction time,molar ratio of alcohol to acid, amount of carrying water agent and repeated uses. Experimental results showed that this catalyst was efficient,economic and easy to use.Under the best conditions the yield could reach 98.6%. |
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| Keywords: | hexyl hexanoate sodium bisulfate catalysis synthesis |
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