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Design and analysis of single-factor experiments: Analysis of variance of the effect of rice husk ash and commercial fillers in NR compounds
Authors:Helson M da Costa  Valéria D Ramos  Leila L Y Visconte  Cristina R G Furtado
Affiliation:(1) Instituto Politécnico – IPRJ, Universidade do Estado do Rio de Janeiro – UERJ, P.O. Box 97282, 28.601-970 Nova Friburgo, RJ, Brasil;(2) Instituto de Macromoléculas Professora Eloisa Mano – IMA, Universidade Federal do Rio de Janeiro – UFRJ, RJ, Brasil;(3) Grupo de Polímeros, Instituto de Química, Universidade do Estado do Rio de Janeiro – UERJ, RJ, Brasil
Abstract:Summary White rice husk ash (WRHA) and black rice husk ash (BRHA) were incorporated into natural rubber (NR) using a laboratory-sized two-roll mill. A conventional vulcanization system was used for curing and physical tests of the NR vulcanized involved determining of tensile and tear resistances. For comparison purposes, precipitated silica (Zeosil-175) and carbon black (N774) were used too. Using the analysis of variance of single-factor experiments, it can be concluded that: BRHA is non-reinforcing filler and its use is limited to 20 phr; WRHA is semi-reinforcing filler and the variation of filler loading (0 up to 50 phr) causes the maximum variation upon tensile strength of NR compounds; and, that although carbon black and silica are reinforcing fillers, a real reinforcement is reached up to 20 phr for tensile strength.
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