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ICP-AES法测定有机肥料中8种元素
引用本文:黄一帆,韦猛,班雁华. ICP-AES法测定有机肥料中8种元素[J]. 现代科学仪器, 2021, 0(2): 60-61,64
作者姓名:黄一帆  韦猛  班雁华
作者单位:广西分析测试研究中心
基金项目:广西分析测试研究中心基本科研项目:(广西地方标准《有机肥料中锰、铁、锌、铜、钙、镁、钾、磷的测定ICP-AES法》的研究)(任务书编号:gxat2019zz03)。
摘    要:目的:建立电感耦合等离子光谱法(ICP-AES)测定有机肥料中营养元素的方法,为科学调查有机肥料中营养元素含量提供技术支持。方法:采用电热板消解方法进行前处理,采用ICP-AES测定锰、铁、锌、铜、钙、镁、钾、磷等8种营养元素在有机肥料样品中的含量。结果:ICP-AES测定8种营养元素的检出限为0.1~13.7mg/kg,精密度为0.9%~2.7%,加标回收率为88.5%~115%。结论:以ICP-AES测定有机肥料中营养元素具有易于操作、选择性好、灵敏度高、定量准确等优势,可在有机肥料营养价值评估中推广应用。

关 键 词:有机肥料  元素  ICP-AES

Determination of eight elements in organic fertilizer by ICP-AES
Huang Yifan,Wei Meng,Ban Yanhua. Determination of eight elements in organic fertilizer by ICP-AES[J]. Modern Scientific Instruments, 2021, 0(2): 60-61,64
Authors:Huang Yifan  Wei Meng  Ban Yanhua
Affiliation:(Guangxi Center for Analysis and Test Research,Nanning,530022)
Abstract:Objective:The inductively coupled plasma atomic emission spectrometry(ICP-AES)method for determining of eight elements in organic fertilizer were established,in order to provide technical supported for scientific investigation of nutrient elements in organic fertilizer.Method:The samples were digested by Electric heating board digestion method.The contents of nutrient elements including Mn,Fe,Zn,Cu,Ca,Mg,K,P in the organic fertilizer samples were determined by ICP-AES.Result:The detection limits 0f eight nutrient elements were 0.1~13.7mg/kg,and the relative standard deviation(RSD)Was 0.9%~2.7%.Recovery was in the range of 88.5%~115%.Conclusion:detennination of nutrient elements in organic fertilizer by ICP-AES has advantages of easy operation,good selectivity,high sensitivity and accuracy.It can be application and dissemination in nutritive value assessment of organic fertilizer.
Keywords:organic fertilizer  element  ICP-AES
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