氧化铟锡/二氧化硅纳米复合纤维膜制备及电化学性能研究 |
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引用本文: | 刘秋美. 氧化铟锡/二氧化硅纳米复合纤维膜制备及电化学性能研究[J]. 中国材料科技与设备, 2012, 0(6): 36-37 |
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作者姓名: | 刘秋美 |
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作者单位: | 贵州大学职业技术学院,贵州贵阳550003 |
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摘 要: | 用溶胶-凝胶法制得了In2O3和SnO2溶胶喷洒在电纺的PVP+正硅酸乙酯纤维薄膜上,在5℃/min升温至550℃,保温3h,随炉冷却至室温,得到分布均匀氧化铟锡/二氧化硅纳米复合纤维膜。大量的试验证明得出:1mL的乙醇中加入0.35mL的正硅酸乙酯的纺丝液的可纺性能最好;用1ml乙醇溶解40mg、50mg、60mg的In2O3,氧化铟锡溶胶喷洒的次数在2—3次时纤维膜的导电性能最好。
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关 键 词: | 喷洒 氧化铟锡 溶胶-凝胶法 电化学性能 |
Indium Tin Oxide/SiO2 Composite Fiber Membrane Nano Preparation and Electrochemical Properties |
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Affiliation: | L IU Qiu --mei (Guizhou University professional technology institute, Guizhou, Guiyang, 550003, China) |
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Abstract: | By sol--gel method and SnO2 sol IreO3got in the electrical spinning spray PVP + teos fiber on film, in 5 ℃ / rain warming to 550 ℃, heat preservation 3 h, along with the furnace cooling to room temperature, get uniform distribution of indium tin oxide/silica nano fiber membrane. A large number of experiments to prove that: 1 mL of ethanol with 0. 35 mL teos spinnahility of the spinning solution performance is the best; With 1 ml ethanol 40 mg dissolved, 50 mg, 60 mg InaO3, indium tin oxide sol the number of spraying in 2-3 times of the conductive fiber membrane performance is the best. |
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Keywords: | Spray Indium tin oxide Sol-gel method Electrochemical performance |
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