| 萘普生中间体的薄层色谱分析 |
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| 引用本文： | 董先明,胡艾希,范国枝. 萘普生中间体的薄层色谱分析[J]. 精细化工中间体, 1999, 0(6) |
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| 作者姓名： | 董先明 胡艾希 范国枝 |
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| 作者单位： | 湖南大学!长沙410082 |
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| 摘 要： | 用薄层色谱法定性分析萘普生合成中的１０ 种中间体， 使用乙酸乙酯∶环己烷＝ １∶４（ Ｖ／ Ｖ） 作展开剂， 在萘普生合成工艺中可用于丙酰基化、溴代和缩酮化等反应进行程度的监测，分析效果好。
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| 关 键 词： | 萘普生 中间体 定性分析 薄层色谱法 |
The Determination of Intermediates in Naproxen Synthesis by TLC |
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| DONG Xianmin HU Aixi FAN Guozhi. The Determination of Intermediates in Naproxen Synthesis by TLC[J]. Fine Chemical Intermediates, 1999, 0(6) |
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| Authors: | DONG Xianmin HU Aixi FAN Guozhi |
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| Affiliation: | Hunan University Changsha 410082 |
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| Abstract: | Ten intermediates in the synthesis of naproxen were analyzed qualitatively by TLC with the mixture of ethyl acetate and cyclohexane as a developping agent. The method has been used to determination of the reaction degree of propionylization, bromination and ketalization in the synthesis of naproxen with satisfied results. |
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| Keywords: | naproxen intermediate qualitative analysis TLC |
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