| 邻硝基对叔丁基苯酚催化加氢研究 |
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| 引用本文： | 吴永忠,王世娟,李玉龙,胡瑾. 邻硝基对叔丁基苯酚催化加氢研究[J]. 广东化工, 2010, 37(12): 198-199,201 |
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| 作者姓名： | 吴永忠 王世娟 李玉龙 胡瑾 |
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| 作者单位： | 南京化工职业技术学院应化系,江苏南京210048 |
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| 摘 要： | 考察了催化剂及其加入量、溶剂及其加入量、反应温度、反应压力对邻硝基对叔丁基苯酚加氢反应的影响。适宜的条件为：催化剂：采用浸渍法制备的自制样，加入量0．10～015g，溶剂：乙醇和正丁醇，优选正丁醇，加入量50mL，反应温度90℃，反应压力0．10MPa。
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| 关 键 词： | 研究 催化加氢 邻硝基对叔丁基苯酚 邻氨基对叔丁基酚 |
Study on the Catalytic Hydrogenation of 2-nitro-4-tert-Butyl-phenol |
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| Wu Yongzhong,Wang Shijuan,Li Yulong,Hu Jin. Study on the Catalytic Hydrogenation of 2-nitro-4-tert-Butyl-phenol[J]. Guangdong Chemical Industry, 2010, 37(12): 198-199,201 |
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| Authors: | Wu Yongzhong Wang Shijuan Li Yulong Hu Jin |
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| Affiliation: | (Department of Applied Chemistry, Nanjing College of Chemical Technology, Nanjing 210048, China) |
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| Abstract: | Influences the kinds of catalyst and its addition amount, the kinds of solvent and its addition amount, the reaction temperature, and the reaction pressure on reaction of 2-nitro-4-tert-butyl-phenol catalytic hydrogenation were investigated. The suitable conditions were catalyst： the homemade catalyst by impregnation, its addition amount： 0.10-0.15 g; solvcnt： ethanol and n-butyl alcohol, optimization to n-butyl alcohol, its addition amount： 50 mL; the reaction temperature： 90 ℃; the reaction prcssure： 0.10 MPa. |
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| Keywords: | study catalytic hydrogenation 2-nitro-4-tcrt-butyl-phenol 2-amino-4-tert-butyl-phenol |
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