液相法制备石墨烯及其摩擦学性能研究 |
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引用本文: | 张伟,朱宏伟,狄泽超,王昆林,吴德海.液相法制备石墨烯及其摩擦学性能研究[J].纳米科技,2011(1):5-9. |
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作者姓名: | 张伟 朱宏伟 狄泽超 王昆林 吴德海 |
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作者单位: | [1]清华大学机械工程系先进成形制造教育部重点实验室,北京100084 [2]中国石油大连润滑油研发中心,辽宁大连116032 |
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摘 要: | 以膨胀石墨为原料,采用液相剥离法和改进Hummers氧化石墨工艺,对氧化石墨进行肼预还原和高温还原,进行了SEM、TEM、Raman以及EDX分析,结果表明,该方法可以制备出微米量级的高质量、高浓度、高产量的石墨烯,又运用SRV试验机检测了石墨烯作为润滑油添加剂的摩擦磨损性能,并对其润滑机理进行探讨。
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关 键 词: | 石墨烯 润滑油 SRV试验机 |
Research on Preparation and Friction Properties of Graphene by Liquid Phase Exfoliation |
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Authors: | ZHANG Wei ZHU Hong-wei DI Ze-chao WANG Kun-lin WU De-hai |
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Affiliation: | 1. Key Laboratory for Advanced Manufacturing by Material Processing Technology and Department of Mechanical Engineering, Tsinghua, Beijing 100084, China) (2. Petrochina Dalian Lubricating Oil R&D Institute, Dalian 116032, China) |
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Abstract: | The expanded graphite as raw material was oxided by liquid stripping method and modified hummers graphite oxide process. And the hydrazine reduction of pre-reduction and high temperature were carried out to graphite oxide and the productions were charactered by SEM, TEM, Raman and EDX analysis. The results indicated that high-quality, high density, high-volume graphene was obtained. The tribological behavior of graphene as lubricant additive is investigated by an oscillating SRV testing machine, and the wear resistance mechanism is discussed. |
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Keywords: | graphene lubricant oscillating SRV apparatus |
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