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氧气-乙炔火焰法制备球形二氧化硅粉体研究
引用本文:杨艳青,许亮,靳洪允.氧气-乙炔火焰法制备球形二氧化硅粉体研究[J].武汉理工大学学报,2011(9).
作者姓名:杨艳青  许亮  靳洪允
作者单位:矿物资源加工与环境湖北省重点实验室;中国地质大学材料科学与化学工程学院;
基金项目:国家青年科学基金(51102218)
摘    要:以天然二氧化硅粉体为原料,采用氧气-乙炔火焰球化法制备球形二氧化硅。实验中选取燃烧气体参数:乙炔流量0.6~0.9m3/h,氧气流量0.8~1.2m3/h。借助XRD衍射仪、扫描电子显微镜对球形化前后样品进行表征,研究了原料粒度、送粉速率对球化效果的影响。结果表明,采用该实验设备和工艺路线可以制备出球化率95%以上的球形二氧化硅,送粉速率越小,原料颗粒粒径越小且粒度分布越均匀(≤10μm),所制备产品的球化率和熔融度越高。

关 键 词:二氧化硅粉  氧气-乙炔火焰  球形化  表征  

Preparation of Spherical Silica Powder by Oxygen-acetylene Flame Method
YANG Yan-qing,XU Liang,JIN Hong-yun.Preparation of Spherical Silica Powder by Oxygen-acetylene Flame Method[J].Journal of Wuhan University of Technology,2011(9).
Authors:YANG Yan-qing  XU Liang  JIN Hong-yun
Affiliation:YANG Yan-qing1,XU Liang2,JIN Hong-yun2 (1.Hubei Key Laboratory of Miner Resources Processing and Environment,Wuhan 430070,China,2.School of Materials Science and Chemical Engineering,China University of Geosciences,Wuhan 430074,China)
Abstract:Spherical silica particles were obtained by the process of heating nature irregularly shaped silica powders under Oxygen-acetylene flame condition.The process variable of preparing spherical silica powder is the flow rate of O2 0.8~1.2 m3/h,the flow rate of C2H2 0.6~0.9 m3/h.The performence of before and after spheroidization powders were characterized by XRD and SEM.The effect of particle size and the feeding rate on spheroidization efficiency were studied.The result showed that after spheroidization,the r...
Keywords:silica power  oxygen-acetylene flame  spheroidization  characterization  
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