| 四氟硼锂和六氟砷锂的合成与拉曼光谱分析 |
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| 引用本文： | 黄力,王德贵.四氟硼锂和六氟砷锂的合成与拉曼光谱分析[J].化学试剂,1996,18(6):366-367. |
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| 作者姓名： | 黄力 王德贵 |
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| 作者单位： | 西北核技术研究所 |
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| 摘 要： | 介绍了合成高纯无水的ＬｉＢＦ４和ＬｉＡｓＦ６的新方法，并讨论了其合成条件，指出制备多孔状ＬｉＦ和控制反应温度是合成的关键。
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| 关 键 词： | 四氟硼锂 六氟砷锂 二次锂电池 拉曼光谱 |
Preparation and Raman spectral analysis of lithium tetrafluoroborate and lithium hexafluoroarsenate |
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| HuangLi,Wang Degui, Zhang Baochuan.Preparation and Raman spectral analysis of lithium tetrafluoroborate and lithium hexafluoroarsenate[J].Chemical Reagents,1996,18(6):366-367. |
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| Authors: | HuangLi Wang Degui Zhang Baochuan |
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| Abstract: | The methods and optimum conditions for thepreparation of LiBF4 and LiAsF6 of high purity werestudied, and it was found that the preparation ofporous, highly reactive LiF and the reaction temperature were the main keys to high yields of the products.From the comparison of the Raman spectrum of theLiBF4 synthesized with that of exotic reference material it was found that the LiBF4 had the same quality.The Raman spectrum of the LiAsF6 produced underthe same conditions is in agreement with that in theliterature. |
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| Keywords: | lithium tetrafluoroborate lithium hexafluoroarsenate rechargeable lithium battery |
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