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牡丹鲜花精油的工业化提取及挥发性组分的GC—MS分析
引用本文:刘俊民,吴震生,朱宗磊,李莹莹,毛文岳. 牡丹鲜花精油的工业化提取及挥发性组分的GC—MS分析[J]. 中国食物与营养, 2014, 0(6): 57-60
作者姓名:刘俊民  吴震生  朱宗磊  李莹莹  毛文岳
作者单位:[1]菏泽尧舜牡丹生物科技有限公司,山东菏泽274000 [2]菏泽学院,山东菏泽274000
摘    要:研究以牡丹鲜花花瓣为原料,采用超临界萃取结合分子蒸馏技术(SFE-MD)方法制备牡丹鲜花精油,并对其挥发性组成成分进行气—质联用(GC-MS)分析和鉴定。结果表明:通过GC-MS分析,可鉴定出牡丹鲜花精油含有95种组分,进一步与图谱库中CAS号相同的组分进行合并,确定了76种组分。其中,牡丹鲜花精油的主要成分共有7种,总含量达74%:分别为樟脑(24.8%、)芳樟醇(20.2%)、松油醇(5.3%)、黄樟脑(6.3%)、反式—橙花叔醇(5.7%)、桉叶油醇(5.3%)、4—萜烯醇(3.0%)。

关 键 词:牡丹花  超临界萃取  牡丹鲜花浸膏  分子蒸馏  牡丹精油

The GC-MS Analysis on Industrial Production and Volatile Compounds of Peony Essential OiL
LIU Jun-min,WU Zhen-sheng,ZHU Zong lei,LI Ying-ying,MAO Wen-yue. The GC-MS Analysis on Industrial Production and Volatile Compounds of Peony Essential OiL[J]. Food and Nutrition in China, 2014, 0(6): 57-60
Authors:LIU Jun-min  WU Zhen-sheng  ZHU Zong lei  LI Ying-ying  MAO Wen-yue
Affiliation:1 Heze rao peony biotechnology co. , LTD. Shandong Heze 274000; 2 Here Uniwersity, Shangdong Here 274000)
Abstract:In this study, peony petal was used as the crude material to prepare essential oil with industrial SFE-MD, and the volatile compounds of essential oil were analyzed and identified by GC-MS. The result showed that, 95 kinds of compounds were detected from essential oil by GC-MS, 76 kinds of which could be confirmed when amalgamated with the compounds labeled the similar CAS number in the data- bases. Furthermore, 7 kinds of compounds, considered as the major components, constituted 74% of the peony essential oil, which were camphor (24. 8% ), linalool (24. 8% ), terpineol ( 15.3% ), yellow camphor (6. 3% ), trans-nerolidol (5.7%), eudesmol (5.3%) and 4-terpene alcohols (3.0%) .
Keywords:peony flower  SFE  extraction of peony flower  MD  peony essential oil
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