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| 固相萃取-气相色谱法检测金银花中9 种拟除虫菊酯农药残留 | |
| 引用本文： | 田丽梅,孙志勇,向 明,宋春满,杨叶昆,李雪梅. 固相萃取-气相色谱法检测金银花中9 种拟除虫菊酯农药残留[J]. 食品科学, 2015, 36(20): 239-241. DOI: 10.7506/spkx1002-6630-201520046 |
| 作者姓名： | 田丽梅 孙志勇 向 明 宋春满 杨叶昆 李雪梅 |
| 作者单位： | 云南中烟工业有限责任公司技术中心，云南 昆明 650106 |
| 基金项目： | 云南中烟工业有限责任公司科技计划项目（2013JC03） |
| 摘 要： | 采用固相萃取净化，气相色谱电子捕获检测器检测，建立了金银花中9 种拟除虫菊酯农药残留量的检测方法。金银花样品经正己烷涡旋振荡提取、TPH固相萃取柱净化后，用气相色谱检测。9 种拟除虫菊酯农药的线性范围在0.01～0.8 mg/L，平均回收率为82.8%～104.6%，相对标准偏差为3.5%～5.7%，检出限为0.002～0.005 mg/L。该方法灵敏、准确，适用于金银花中9 种拟除虫菊酯类农药残留量分析。 |
| 关 键 词： | 气相色谱 固相萃取 拟除虫菊酯 农药残留 金银花 |
Determination of 9 Pyrethroid Pesticide Residues in Honeysuckle by Solid Phase Extraction and Gas Chromatography |
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| TIAN Limei,SUN Zhiyong,XIANG Ming,SONG Chunman,YANG Yekun,LI Xuemei. Determination of 9 Pyrethroid Pesticide Residues in Honeysuckle by Solid Phase Extraction and Gas Chromatography[J]. Food Science, 2015, 36(20): 239-241. DOI: 10.7506/spkx1002-6630-201520046 | |
| Authors: | TIAN Limei SUN Zhiyong XIANG Ming SONG Chunman YANG Yekun LI Xuemei |
| Affiliation: | Technology Center, China Tobacco Yunnan Industrial Co. Ltd., Kunming 650106, China |
| Abstract: | A method was developed for the determination of 9 pyrethroid pesticide residues in honeysuckle with solidphase extraction and gas chromatography. The results showed that average recoveries of 9 pesticides spiked at 0.02, 0.1 and 0.5 μg/g were in the range of 82.8%–104.6% with relative standard deviation (RSD) of 3.5%–5.7%. The linear range of the presented method was 0.01–0.8 mg/L, and the limits of detection (LOD) were 0.002–0.005 mg/L. The method is sensitive and suitable for the analysis of pyrethroid pesticide residues in honeysuckle. |
| Keywords: | gas chromatography solid-phase extraction pyrethroid pesticide residue honeysuckle |
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