| 氯气氧化法合成四氯苯醌的研究 |
| |
| 引用本文： | 陈小明. 氯气氧化法合成四氯苯醌的研究[J]. 广东化工, 2012, 39(14): 65-65,52 |
| |
| 作者姓名： | 陈小明 |
| |
| 作者单位： | 江苏省泰兴市中等专业擎校经贸化工系,江苏泰兴,225400 |
| |
| 摘 要： | 以对苯二酚、氯气、冰醋酸、盐酸为原料,以醋酸与盐酸混合物(比例为6∶1)为溶剂,两釜串联通氯,三釜循环使用,阶段式程序自动升温反应,氯气使用量分三段程序变化,合成四氯苯醌,合成四氯苯醌的收率达到98%,纯度达到99%。
|
| 关 键 词： | 四氯苯醌 氯气 新工艺 |
Chlorine Oxidation Process for Synthesizing Chloranil Research |
| |
| Chen Xiaoming. Chlorine Oxidation Process for Synthesizing Chloranil Research[J]. Guangdong Chemical Industry, 2012, 39(14): 65-65,52 |
| |
| Authors: | Chen Xiaoming |
| |
| Affiliation: | Chen Xiaoming(Economic and Trade Department of Chemical Engineering,Jiangsu province Taixing city secondary school,Taixing 225400,China) |
| |
| Abstract: | With hydroquinone,chlorine,hydrochloric acid,acetic acid,acetic acid and hydrochloric acid in the mixture（ratio of 6∶1） as solvent,two kettle series connection to chlorine,three kettle for recycling,staged procedures for automatic temperature reaction,chlorine using volume three section four chloranil program changes,synthesis,synthesis of four chlorine by the yield was 98 %,99 % purity. |
| |
| Keywords: | chloranil chlorine new technology |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
