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Sn~(4+)取代对NiZn功率铁氧体磁性能的影响
引用本文:马玉启,刘先松,冯双久,黄鑫,黄风.Sn~(4+)取代对NiZn功率铁氧体磁性能的影响[J].材料工程,2015(8):72-76.
作者姓名:马玉启  刘先松  冯双久  黄鑫  黄风
作者单位:安徽大学物理与材料科学学院磁性材料安徽省工程技术研究中心,合肥,230601
基金项目:国家自然科学基金资助项目(51072002,51272003);安徽省教育厅重点科研项目资助(KJ2010A008,KJ2012A027);2013年度安徽省级自然科学研究项目资助(K J2013B293);高等学校博士学科点专项科研基金资助
摘    要:采用固相反应法制备化学计量为Ni0.65Zn0.35SnxFe2-xO4(x=0.00~0.08)的铁氧体软磁材料。采用XRD、SEM、LCR测试仪、B-H分析仪对其结构、电磁性能进行研究。结果表明:随Sn4+取代量x的增加,晶格常数a逐渐增大,晶粒尺寸变化不大,饱和磁通密度Bs逐渐下降,铁氧体的起始磁导率μi先上升后下降,功率损耗Pcv与μi的变化呈相反趋势。当Sn4+的取代量x=0.04时具有最低的功率损耗,且Pcv随着温度的升高而逐渐降低。

关 键 词:NiZn功率铁氧体  Sn4%2B取代  起始磁导率  功率损耗

Influence of Sn4+ Substitution on M agnetic Properties of NiZn Pow er Ferrites
MA Yu-qi,LIU Xian-song,FENG Shuang-jiu,HUANG Xin,HUANG Feng.Influence of Sn4+ Substitution on M agnetic Properties of NiZn Pow er Ferrites[J].Journal of Materials Engineering,2015(8):72-76.
Authors:MA Yu-qi  LIU Xian-song  FENG Shuang-jiu  HUANG Xin  HUANG Feng
Abstract:The stoichiometric Ni0.65Zn0.35SnxFe2 - xO4(x=0 .00‐0 .08) power ferrites soft magnetic ma‐terial was prepared by the solid‐state reaction method .The structural characteristics and electromag‐netic properties were investigated by X‐ray diffraction(XRD) ,SEM ,LCR tester ,B‐H analyzer ,respec‐tively .The results indicate that with increasing Sn4+ substitution amount ,lattice constant a increases gradually ,grain size varies not much ,saturation magnetic flux density Bs continuously decreases ,ini‐tial permeability μi of the ferrites increases initially and then decreases ,and pow er loss Pcv has an op‐posite change with μi .The power loss Pcv has a minimum value when the Sn4+ substitution amount is 0 .04 and Pcv decreases gradually w hen the temperature increases .
Keywords:NiZn power ferrites  Sn4+ substitution  initial permeability  power loss
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