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基于原位和RNT技术的摩擦试验机及其实验研究
引用本文:刘麟,张志臣,詹普杰,Martin Dienwiebel. 基于原位和RNT技术的摩擦试验机及其实验研究[J]. 仪器仪表学报, 2016, 37(12): 2873-2879
作者姓名:刘麟  张志臣  詹普杰  Martin Dienwiebel
作者单位:常州大学机械工程学院常州213164,常州大学机械工程学院常州213164,常州大学机械工程学院常州213164,2. 卡尔斯鲁厄理工学院 应用材料研究所卡尔斯鲁厄76128;3. 弗劳恩霍夫应用技术研究协会 材料力学研究所弗莱堡79108
基金项目:国家自然科学基金(51601021,51441001)、江苏省自然科学基金(BK20140262)、江苏省高校自然科学研究(14KJB460001)项目资助
摘    要:针对目前传统摩擦磨损试验机的不足之处,开发了一种基于原位和RNT技术的摩擦磨损试验机。在合理设计和选取试验机工作系统及主要部件的基础上,采用原位全息显微技术和放射性核素技术,实现了对摩擦过程中材料磨痕表面微观形貌的在线原位观察和磨损量的实时精确测量。利用试验机对CuZ n20/100Cr6进行摩擦磨损性能实验,并对试验后试样进行了X射线电子能谱分析(XPS)、扫描电子显微镜(SEM)和透射电子显微镜(TEM)分析研究。结果表明,磨痕表面形成耐磨层和晶粒细化是CuZ n20具有良好耐磨性的主要原因;试验机的实验结果精确,能为深入研究材料摩擦学行为提供重要参考依据。

关 键 词:摩擦试验机;原位全息显微技术;放射性核素技术;铜锌合金

Tribometer based on in situ and radionuclide technique and its characteristic experiment study
Liu Lin,Zhang Zhichen,Zhan Pujie and Martin Dienwiebel. Tribometer based on in situ and radionuclide technique and its characteristic experiment study[J]. Chinese Journal of Scientific Instrument, 2016, 37(12): 2873-2879
Authors:Liu Lin  Zhang Zhichen  Zhan Pujie  Martin Dienwiebel
Abstract:Aiming at the deficiencies of traditional tribometers, a new tribometer based on in situ and radionuclide techniques is developed in this paper. The working system and main components of the tribometer were designed and selected reasonably, based on which the in situ holographic microscopy and radionuclide techniques were applied in the tribometer to realize the on line in situ observation of the microstructure of the material grinding crack surface in the friction process and the accurate real time measurement of the wearing loss. The friction and wearing behavior experiments of the brass samples (i.e. 80% of copper and 20% of zinc) sliding against 100 of Cr6 under lubricated condition were conducted on the developed tribometer, and the samples were analyzed and studied with XPS, SEM and TEM after the experiments. The results indicate that the oxide layer formed on the grinding crack surface and the crystal grain refinement during the experiments are the main reasons for good wearing resistance of the brass sample. The experiment results obtained with the tribometer are accurate, which provides an important reference basis for deeply studying the tribological behaviors of materials.
Keywords:tribometer   in situ holographic microscopy technique   radionuclide technique   copper zinc alloy
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