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Sm2Co17型永磁材料金相样品的腐蚀条件研究
引用本文:赖维明,包生祥,张晓雯,王祖文,程玲莉,张明.Sm2Co17型永磁材料金相样品的腐蚀条件研究[J].磁性材料及器件,2012,43(4):63-65.
作者姓名:赖维明  包生祥  张晓雯  王祖文  程玲莉  张明
作者单位:1. 电子科技大学 电子薄膜与集成器件国家重点实验室,四川成都,610054
2. 中国国防科技信息中心,北京,100142
3. 西南应用磁学研究所,四川绵阳,621000
基金项目:总装备部军用电子元器件"共性与支撑"项目
摘    要:用三种金相腐蚀剂和不同的腐蚀时间对Sm2Co17型永磁材料进行腐蚀,通过扫描电子显微镜(SEM)结合X射线能谱仪(EDS)对Sm2Co17型永磁材料的金相腐蚀条件进行了研究.结果表明,0.5ml硝酸、2ml乙酸、100ml蒸馏水的配比,腐蚀60s能清晰显示晶界、晶粒表面以及晶粒中的富Zr和富Sm析出相.与最常用金属材料...

关 键 词:Sm2Co17永磁材料  扫描电镜  金相腐蚀  腐蚀条件

Studies on corrosion conditions of metallographic sample of Sm2Co17 permanent magnet materials
LAI Wei-ming , BAO Sheng-xiang , ZHANG Xiao-wen , WANG Zu-wen , CHENG Lin-li , ZHANG Ming.Studies on corrosion conditions of metallographic sample of Sm2Co17 permanent magnet materials[J].Journal of Magnetic Materials and Devices,2012,43(4):63-65.
Authors:LAI Wei-ming  BAO Sheng-xiang  ZHANG Xiao-wen  WANG Zu-wen  CHENG Lin-li  ZHANG Ming
Affiliation:1.State Key Laboratory of Electronic Thin Films and Integrated Devices,University of Electronic Science and Technology of China,Chengdu 610054,China;2.China National Defense Science and Technology Information Center,Beijing 100142;3.Southwest Institute of Applied Magnetics,Mianyang 621000,China
Abstract:Sm2Co17 type permanent magnet materials were corroded under three kinds of corrosion conditions.Scanning electron microscopy and energy dispersive X-ray spectrometer were used to study the metallographic corrosion conditions.The result showed that sample corroded for 60 seconds in corrosive liquid of 100ml distilled water dissoled in 0.5ml nitric acid and 2ml acetic acid can clearly display boundary,surface of grain,and Zr-rich and Sm-rich phase in the grain.Compared with the corrosion agent most commonly used to metal material and the formula from metallographic corrosion handbook,the corrosion agent determined in this research can get a more clearly metallographic image.
Keywords:Sm2Co17permanent magnet materials  scanning electron microscopy  metallographic corrosion  corrosion conditions
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