Characterization of Bi2S3 nanorods and nano-structured flowers prepared by a hydrothermal method |
| |
| Authors: | Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem |
| |
| Affiliation: | a Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200, Thailand
b Department of Chemistry, Faculty of Science, Chiang Mai University, Chiang Mai 50200, Thailand |
| |
| Abstract: | Bismuth sulfide nanorods and nano-structured flowers were synthesized by hydrothermal reaction of bismuth nitrate pentahydrate and thiourea solutions, containing 1 and 2 ml of 65% HNO3, respectively. By using X-ray diffraction (XRD), selected area electron diffraction (SAED), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM) and high resolution TEM (HRTEM), the products were specified as orthorhombic Bi2S3 in the shapes of nanorods and flower-like clusters of nanorods, with the growth of nanorods in the 001] direction. A diffraction pattern was also simulated, and was in good accordance with the SAED pattern obtained from the experiment. |
| |
| Keywords: | Bismuth sulfide Nanorods Nano-structured flowers Hydrothermal method |
| 本文献已被 ScienceDirect 等数据库收录！ |
|
