| 氯化铁催化合成乙酸异戊酯工艺研究 |
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| 引用本文： | 廖德仲,许凌.氯化铁催化合成乙酸异戊酯工艺研究[J].精细石油化工,1996(5):43-45. |
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| 作者姓名： | 廖德仲 许凌 |
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| 作者单位： | 岳阳大学化工系!414000 |
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| 摘 要： | 研究了氯化铁催化合成乙酸异戊酯的工艺条件 ,在优化条件下 ,乙酸异戊酯的收率超过 95%。优化条件如下 :异戊醇 0 .3 mol;乙酸 0 .36mol;反应时间 1 h;反应温度 1 4 5± 2℃ ;氯化铁 0 .88g。并提出了反应的可能机理。
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| 关 键 词： | 氯化铁 催化 乙酸异戊酯 机理 |
A STUDY ON SYNTHESIS OF ISOAMYL ACETATE BY CATALYSIS OF FERRIC CHLORIDE |
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| Liao Dezhong and Xu Ling.A STUDY ON SYNTHESIS OF ISOAMYL ACETATE BY CATALYSIS OF FERRIC CHLORIDE[J].Speciality Petrochemicals,1996(5):43-45. |
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| Authors: | Liao Dezhong and Xu Ling |
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| Abstract: | In this paper the synthetic condition of isoamyl acetate by catalysis of ferric chloride was studied. In the optimun condition, the yield is above 95%. The optimun condition is as follows: isoamyl alcohol 0.3mol; acetic acid 0.36mol;reaction time 1h; reation temperature 145±2℃; ferric chloride 0.88g, and the possible catalytic mechanism is illustrated. |
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| Keywords: | ferric chloride catalysis isoamyl acetate mechanism |
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