Solvothermal Synthesis and Crystal Structure of a Novel 3D Triorganotin Polymer Containing Polyfunctional Ligand 5-mercapto-1(H)-tetrazoleacetic acid |
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| Authors: | Chunlin Ma Qingfeng Wang Rufen Zhang |
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| Affiliation: | (1) Department of Chemistry, Liaocheng University, 252059 Liaocheng, People’s Republic of China;(2) Department of Chemistry, Taishan University, 271021 Taian, People’s Republic of China |
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| Abstract: | A novel 3D tri-n-butyltin complex [(n-Bu3Sn)2(C2H2N4SCO2)]n (1) has been solvothermally synthesized and structurally characterized by elemental analysis, FT-IR, NMR (1H, 13C, and 119Sn) spectra and X-ray crystallography. X-ray data of complex 1 reveals that it is a 3D tri-n-butyltin coordination polymer with a metal-organic framework (MOF) structure , significant N → Sn interactions plays an important role in the construction of this structure. |
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| Keywords: | 5-Mercapto-1(H)-tetrazoleacetic acid Tri-n-butyltin chloride Solvothermally condition |
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