| 正丁醇铝的制备及其水解 |
| |
| 引用本文： | 丑修建,郭旭侠,王洁,陈庆华. 正丁醇铝的制备及其水解[J]. 云南化工, 2004, 31(2): 1-3,6 |
| |
| 作者姓名： | 丑修建 郭旭侠 王洁 陈庆华 |
| |
| 作者单位： | 1. 昆明理工大学材料与冶金工程学院,云南 昆明 650093
2. 昆明理工大学环境工程学院,云南 昆明 650093 |
| |
| 基金项目： | 云南省二层次人才培养资助项目(20034). |
| |
| 摘 要： | 主要研究了正丁醇铝的制备及其水解,通过IR、DSC/TG和XRD测试手段分析,结果表明:采用醇解法可以有效制备正丁醇铝,控制水解温度和水解配比,能够获得高质量的氧化铝溶胶,铝溶胶热处理到600～800℃之间为γ Al2O3,热处理到1200℃为α Al2O3。
|
| 关 键 词： | 正丁醇铝 溶胶凝胶法 水解 氧化铝 |
| 文章编号： | 1004-275X(2004)02-0001-03 |
Preparation and Hydrolysis of Aluminum Butanoxide |
| |
| CHOU Xiu-jian,GUO Xu-xia,WANG Jie,CHEN Qing-hua. Preparation and Hydrolysis of Aluminum Butanoxide[J]. Yunnan Chemical Technology, 2004, 31(2): 1-3,6 |
| |
| Authors: | CHOU Xiu-jian GUO Xu-xia WANG Jie CHEN Qing-hua |
| |
| Affiliation: | CHOU Xiu-jian~1,GUO Xu-xia~1,WANG Jie~2,CHEN Qing-hua~1 |
| |
| Abstract: | Preparation and hydrolysis of aluminum butanoxide were studied. Result on the analysis of IR, DSC/TG and XRD showed that it could be prepared effectively by alcoholysis and high quality of alumina sol could be obtained by the control of hydrolysis temperature and ratio. γ-alumina could be acquired when alumina sol was heated between 600 to 800℃ and α-alumina prepared when heated at?1?200℃. |
| |
| Keywords: | aluminum butanoxide sol-gel hydrolysis alumina |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
