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食品中氯酸盐和高氯酸盐分析方法综述
引用本文:宋 瑞,李清清,陆志芸.食品中氯酸盐和高氯酸盐分析方法综述[J].食品安全质量检测技术,2019,10(21):7115-7120.
作者姓名:宋 瑞  李清清  陆志芸
作者单位:上海市质量监督检验技术研究院,上海市质量监督检验技术研究院,上海市质量监督检验技术研究院
基金项目:上海市市场监测管理局科技项目 (2018-34)
摘    要:高氯酸盐是一种新型环境污染物, 具有高扩散性和持久性, 它可以干扰人体甲状腺的正常功能, 从而影响人体生长发育。食品中氯酸盐和高氯酸盐的测定对于保证人体健康有重要意义, 也是目前国际国内研究的热点问题。目前国内外已有多种分析方法实现了对氯酸盐和高氯酸盐定量检测, 主要包括离子色谱法、离子色谱-质谱法、液相色谱-质谱法等。本文对近年来食品中氯酸盐和高氯酸盐分析检测方法的研究情况进行整理, 对各种分析技术的原理、应用现状及国内外相关标准进行探讨, 对其优缺点进行了比较, 并提出了前景展望。

关 键 词:氯酸盐    高氯酸盐    离子色谱法    离子色谱-质谱法    液相色谱-质谱法
收稿时间:2019/9/24 0:00:00
修稿时间:2019/10/27 0:00:00

Discussion on analytical method of chlorate and perchlorate in food
SONG Rui,LI Qing-Qing and LU Zhi-Yun.Discussion on analytical method of chlorate and perchlorate in food[J].Food Safety and Quality Detection Technology,2019,10(21):7115-7120.
Authors:SONG Rui  LI Qing-Qing and LU Zhi-Yun
Affiliation:Shanghai Institute of Quality Inspection and Technical Research,Shanghai Institute of Quality Inspection and Technical Research and Shanghai Institute of Quality Inspection and Technical Research
Abstract:Perchlorate is a new type of environmental pollutant with high diffusivity and durability. It can interfere with the normal function of the human thyroid gland and affect human growth and development. The determination of chlorate and perchlorate in food is of great significance for ensuring human health, and it is also a hot issue in international and domestic research. At present, there are various analytical methods at home and abroad to achieve quantitative detection of chlorate and perchlorate, including ion chromatography, ion chromatography- mass spectrometry, liquid chromatography-mass spectrometry. This paper reviewed the research status of chlorate and perchlorate analysis and detection methods in foods in recent years, discussed the principles, application status and relevant standards of various analytical techniques, compared their advantages and disadvantages and put forward the prospects.
Keywords:chlorate  perchlorate  ion chromatography  ion chromatography-mass spectrometry  liquid chromatography- mass spectrometry
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